p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranoside

Base Information

Chemical Name:p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranoside
CAS No.:664998-12-3
Molecular Formula:C₁₇H₂₃N₃O₆
Molecular Weight:365.386
Hs Code.:

Synonyms:p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranoside

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Technology Process of p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranoside

There total 1 articles about p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: p-methoxybenzyl 2-azido-2-deoxy-6-O-tert-butyldiphenylsilyl-3,4-O-isopropylidene-D-galactopyranoside

: 664998-12-3
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranoside

: 664997-97-1
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1039/b307674a

Reference yield: 94.0%

: 664998-12-3
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranoside

: 664998-08-7
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 25 ℃; for 1h;
DOI:10.1039/b307674a

Reference yield:

: 664998-12-3
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranoside

: 664998-09-8
3-(4-methoxybenzyl)-1-[p-methoxybenzyl (11R)-2-azido-2,7-dideoxy-3,4:9,10-di-O-isopropylidene-6-keto-L-ribo-β-D-galacto-undecodialdo-1,5-pyranoside-11,8-furanosyl]uracil

Guidance literature:: Multi-step reaction with 2 steps

1.1: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h / 25 °C

2.1: aq. KOH / methanol; diethyl ether / 0.08 h / 0 °C

2.2: 60 percent / diethyl ether / 1 h / 0 °C

With potassium hydroxide; Dess-Martin periodane; In methanol; diethyl ether; dichloromethane;
DOI:10.1039/b307674a