p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside

Base Information

Chemical Name:p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside
CAS No.:664998-08-7
Molecular Formula:C₁₇H₂₁N₃O₆
Molecular Weight:363.37
Hs Code.:

Synonyms:p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside

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Chemical Property of p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside

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Technology Process of p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside

There total 2 articles about p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 664998-12-3
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galactopyranoside

: 664998-08-7
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 25 ℃; for 1h;
DOI:10.1039/b307674a

Reference yield:

: p-methoxybenzyl 2-azido-2-deoxy-6-O-tert-butyldiphenylsilyl-3,4-O-isopropylidene-D-galactopyranoside

: 664998-08-7
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / TBAF / tetrahydrofuran / 1 h / 0 °C

2: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h / 25 °C

With tetrabutyl ammonium fluoride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b307674a

Reference yield: 60.0%

: 664998-08-7
p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside

: 664998-07-6
1-(5-(N-nitroso)-acetamido-5-deoxy-2,3-O-isopropylidene-β-D-ribofuranosyl)-3-(4-methoxybenzyl)uracil

: 664998-09-8
3-(4-methoxybenzyl)-1-[p-methoxybenzyl (11R)-2-azido-2,7-dideoxy-3,4:9,10-di-O-isopropylidene-6-keto-L-ribo-β-D-galacto-undecodialdo-1,5-pyranoside-11,8-furanosyl]uracil

Guidance literature:: 1-(5-(N-nitroso)-acetamido-5-deoxy-2,3-O-isopropylidene-β-D-ribofuranosyl)-3-(4-methoxybenzyl)uracil; With potassium hydroxide; In methanol; diethyl ether; at 0 ℃; for 0.0833333h;

p-methoxybenzyl 2-azido-2-deoxy-3,4-O-isopropylidene-β-D-galacto-hexonodialdo-1,5-pyranoside; In diethyl ether; at 0 ℃; for 1h; Further stages.;
DOI:10.1039/b307674a