(S)-1-((1,1-dibromo-4-methylocta-1,7-dien-4-yloxy)methyl)-4-methoxybenzene

Base Information

Chemical Name:(S)-1-((1,1-dibromo-4-methylocta-1,7-dien-4-yloxy)methyl)-4-methoxybenzene
CAS No.:949087-77-8
Molecular Formula:C₁₇H₂₂Br₂O₂
Molecular Weight:418.168
Hs Code.:

Synonyms:(S)-1-((1,1-dibromo-4-methylocta-1,7-dien-4-yloxy)methyl)-4-methoxybenzene

Suppliers and Price of (S)-1-((1,1-dibromo-4-methylocta-1,7-dien-4-yloxy)methyl)-4-methoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-1-((1,1-dibromo-4-methylocta-1,7-dien-4-yloxy)methyl)-4-methoxybenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-1-((1,1-dibromo-4-methylocta-1,7-dien-4-yloxy)methyl)-4-methoxybenzene

There total 3 articles about (S)-1-((1,1-dibromo-4-methylocta-1,7-dien-4-yloxy)methyl)-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 949087-76-7
(S)-3-(4-methoxybenzyloxy)-3-methylhept-6-enal

: 558-13-4
carbon tetrabromide

: 949087-77-8
(S)-1-((1,1-dibromo-4-methylocta-1,7-dien-4-yloxy)methyl)-4-methoxybenzene

Guidance literature:: carbon tetrabromide; With triphenylphosphine; In dichloromethane; at 20 ℃; for 0.5h;

(S)-3-(4-methoxybenzyloxy)-3-methylhept-6-enal; With triethylamine; In dichloromethane; at -78 - 20 ℃; for 13h; Further stages.;
DOI:10.1021/jo070709p

Reference yield:

: 949087-75-6
(4S)-4-(but-3-enyl)-2-(4-methoxyphenyl)-4-methyl-1,3-dioxane

: 949087-77-8
(S)-1-((1,1-dibromo-4-methylocta-1,7-dien-4-yloxy)methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 76 percent / DIBAL-H / CH₂Cl₂; toluene / 2 h / -20 °C

2.1: oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -78 - 20 °C

3.1: PPh₃ / CH₂Cl₂ / 0.5 h / 20 °C

3.2: 2.47 g / NEt₃ / CH₂Cl₂ / 13 h / -78 - 20 °C

With oxalyl dichloride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; In dichloromethane; toluene;
DOI:10.1021/jo070709p

Reference yield:

: 949087-70-1
(S)-3-(4-methoxybenzyloxy)-3-methylhept-6-en-1-ol

: 949087-77-8
(S)-1-((1,1-dibromo-4-methylocta-1,7-dien-4-yloxy)methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -78 - 20 °C

2.1: PPh₃ / CH₂Cl₂ / 0.5 h / 20 °C

2.2: 2.47 g / NEt₃ / CH₂Cl₂ / 13 h / -78 - 20 °C

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; triphenylphosphine; In dichloromethane;
DOI:10.1021/jo070709p