C₁₂H₁₂ClN₃O₃

Base Information

Chemical Name:C₁₂H₁₂ClN₃O₃
CAS No.:1374986-13-6
Molecular Formula:C₁₂H₁₂ClN₃O₃
Molecular Weight:281.699
Hs Code.:

C<sub>12</sub>H<sub>12</sub>ClN<sub>3</sub>O<sub>3</sub>

Synonyms:C₁₂H₁₂ClN₃O₃

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Chemical Property of C₁₂H₁₂ClN₃O₃

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Technology Process of C₁₂H₁₂ClN₃O₃

There total 3 articles about C₁₂H₁₂ClN₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.1%

: 1374986-05-6
methyl-5-chloroisoxazolo[4,5-b]pyrazine-3-carboxylate

: 108-93-0
cyclohexanol

: 1374986-13-6
C₁₂H₁₂ClN₃O₃

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; at 100 ℃; for 1h;

Reference yield:

: C₁₁H₁₅N₂O₆^(1-)*K⁽¹⁺⁾

: 1374986-13-6
C₁₂H₁₂ClN₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid; hydroxylamine hydrochloride / methanol / 5 h / 10 °C / Inert atmosphere; Reflux

2: toluene-4-sulfonic acid; acetic acid / 2 h / 77 - 80 °C / Industrial scale

3: trichlorophosphate; triethylamine hydrochloride / 4 h / 85 °C

4: N-ethyl-N,N-diisopropylamine; dmap / 1 h / 100 °C

With dmap; hydroxylamine hydrochloride; triethylamine hydrochloride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; trichlorophosphate; In methanol;

Reference yield:

: 1374986-04-5
C₇H₅N₃O₄

: 1374986-13-6
C₁₂H₁₂ClN₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate; triethylamine hydrochloride / 4 h / 85 °C

2: N-ethyl-N,N-diisopropylamine; dmap / 1 h / 100 °C

With dmap; triethylamine hydrochloride; N-ethyl-N,N-diisopropylamine; trichlorophosphate;