(2R)-1-[(Z)-{[2-(allyloxy)-1-naphthyl]methylene}(oxido)amino]-2-phenylethanol

Base Information

Chemical Name:(2R)-1-[(Z)-{[2-(allyloxy)-1-naphthyl]methylene}(oxido)amino]-2-phenylethanol
CAS No.:436806-96-1
Molecular Formula:C₂₂H₂₁NO₃
Molecular Weight:347.414
Hs Code.:

Synonyms:(2R)-1-[(Z)-{[2-(allyloxy)-1-naphthyl]methylene}(oxido)amino]-2-phenylethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-1-[(Z)-{[2-(allyloxy)-1-naphthyl]methylene}(oxido)amino]-2-phenylethanol

Chemical Property:

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Technology Process of (2R)-1-[(Z)-{[2-(allyloxy)-1-naphthyl]methylene}(oxido)amino]-2-phenylethanol

There total 1 articles about (2R)-1-[(Z)-{[2-(allyloxy)-1-naphthyl]methylene}(oxido)amino]-2-phenylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 19530-43-9
2-allyloxy-1-naphthaldehyde

: 321174-47-4
(R)-α-(hydroxymethyl)benzylhydroxylamine

: 436806-96-1
(2R)-1-[(Z)-{[2-(allyloxy)-1-naphthyl]methylene}(oxido)amino]-2-phenylethanol

Guidance literature:: With magnesium sulfate; acetic acid; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/jo011015y

Reference yield: 89.0%

: 436806-96-1
(2R)-1-[(Z)-{[2-(allyloxy)-1-naphthyl]methylene}(oxido)amino]-2-phenylethanol

: (2R)-2-((3aR,11cS)-3a,11c-dihydro-3H-benzo[5,6]chromeno[4,3-c]isoxazol-1(4H)-yl)-2-phenylethanol

: 436807-00-0
(2R)-2-((3aS,11cR)-3a,11c-dihydro-3H-benzo[5,6]chromeno[4,3-c]isoxazol-1(4H)-yl)-2-phenylethanol

Guidance literature:: With zinc trifluoromethanesulfonate; triethylamine; In dichloromethane; at 40 ℃; for 68h;
DOI:10.1021/jo011015y

Reference yield:

: 436806-96-1
(2R)-1-[(Z)-{[2-(allyloxy)-1-naphthyl]methylene}(oxido)amino]-2-phenylethanol

: 321574-22-5
N-[(1R,2R)-2-(hydroxymethyl)-2,3-dihydro-1H-benzo[f]chromen-1-yl]-N-methyl-N'-[3-(trifluoromethyl)phenyl]thiourea

Guidance literature:: Multi-step reaction with 5 steps

1.1: Bu₂BOTf; Et₃N / CH₂Cl₂ / 68 h / 40 °C

2.1: methanesulfonyl chloride; Et₃N / CH₂Cl₂ / 3 h / 20 °C

2.2: KH / 2-methyl-propan-2-ol / 18 h / 40 °C

2.3: 85 percent / aq. HCl / tetrahydrofuran / 6 h

3.1: 92 percent / Zn; aq. AcOH / tetrahydrofuran / 55 °C

4.1: Et₃N / tetrahydrofuran / 2 h / 20 °C

4.2: 88 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

5.1: 95 percent / tetrahydrofuran / 15 h / 20 °C

With di-n-butylboryl trifluoromethanesulfonate; acetic acid; methanesulfonyl chloride; triethylamine; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo011015y