β-(R)-phenyl-2-(R)-piperidineethanol

Base Information

Chemical Name:β-(R)-phenyl-2-(R)-piperidineethanol
CAS No.:220858-75-3
Molecular Formula:C₁₃H₁₉NO
Molecular Weight:205.3
Hs Code.:

Synonyms:β-(R)-phenyl-2-(R)-piperidineethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-(R)-phenyl-2-(R)-piperidineethanol

Chemical Property:

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Technology Process of β-(R)-phenyl-2-(R)-piperidineethanol

There total 6 articles about β-(R)-phenyl-2-(R)-piperidineethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 220858-74-2
β-(R)-phenyl-1-(phenylmethyl)-2-(R)-piperidineethanol

: 220858-75-3
β-(R)-phenyl-2-(R)-piperidineethanol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 4h; under 2585.74 Torr; Ambient temperature;
DOI:10.1021/jo9821473

Reference yield:

: 103-82-2
phenylacetic acid

: 220858-75-3
β-(R)-phenyl-2-(R)-piperidineethanol

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / pivaloyl chloride, triethylamine / toluene

3: 93 percent / triethylamine / toluene / 2 h / 0 °C

4: 91 percent / NaBH₄ / tetrahydrofuran; H₂O / 0 - 22 °C

5: 60 percent / 3 h / 85 °C

6: hydrogen / Pd/C / ethanol / 4 h / 2585.74 Torr / Ambient temperature

With sodium tetrahydroborate; hydrogen; pivaloyl chloride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; toluene;
DOI:10.1021/jo9821473

Reference yield:

: 161745-73-9
(4R)-3-phenylacetyl-4-phenyl-1,3-oxazolidin-2-one

: 220858-75-3
β-(R)-phenyl-2-(R)-piperidineethanol

Guidance literature:: Multi-step reaction with 5 steps

2: 93 percent / triethylamine / toluene / 2 h / 0 °C

3: 91 percent / NaBH₄ / tetrahydrofuran; H₂O / 0 - 22 °C

4: 60 percent / 3 h / 85 °C

5: hydrogen / Pd/C / ethanol / 4 h / 2585.74 Torr / Ambient temperature

With sodium tetrahydroborate; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; toluene;
DOI:10.1021/jo9821473