tert-butyl 4-acetylphenyl(3-perfluorooctylpropoxy)carbamate

Base Information

• Chemical Name: tert-butyl 4-acetylphenyl(3-perfluorooctylpropoxy)carbamate
• CAS No.: 1239374-09-4
• Molecular Formula: C₂₄H₂₂F₁₇NO₄
• Molecular Weight: 711.416
• Mol file: 1239374-09-4.mol

Synonyms:tert-butyl 4-acetylphenyl(3-perfluorooctylpropoxy)carbamate

Chemical Property of tert-butyl 4-acetylphenyl(3-perfluorooctylpropoxy)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of tert-butyl 4-acetylphenyl(3-perfluorooctylpropoxy)carbamate

There total 1 articles about tert-butyl 4-acetylphenyl(3-perfluorooctylpropoxy)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Iodoacetophenone (13329-40-3) + tert-butyl (3-perfluorooctyl)propoxycarbamate (1228692-98-5) → tert-butyl 4-acetylphenyl(3-perfluorooctylpropoxy)carbamate (1239374-09-4)

Guidance literature:

With copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine; In toluene; at 110 ℃; for 16h; Inert atmosphere;

DOI:10.1002/ejoc.201000367

Reference yield: 100.0%

tert-butyl 4-acetylphenyl(3-perfluorooctylpropoxy)carbamate (1239374-09-4) → tert-butyl 4-acetylphenylcarbamate (232597-42-1)

Guidance literature:

With methanol; tris(propionitrile)tricarbonylmolybdenum⁽⁰⁾; at 130 ℃; for 0.25h; chemoselective reaction; Microwave irradiation; Inert atmosphere;

DOI:10.1002/ejoc.201000367

upstream raw materials:

4-Iodoacetophenone

tert-butyl (3-perfluorooctyl)propoxycarbamate

Downstream raw materials:

tert-butyl 4-acetylphenylcarbamate