N’-(2-((2,4-dimethoxybenzyl)amino)-8-methylquinazolin-4-yl)-2-hydroxyacetohydrazide

Base Information

Chemical Name:N’-(2-((2,4-dimethoxybenzyl)amino)-8-methylquinazolin-4-yl)-2-hydroxyacetohydrazide
CAS No.:1616709-21-7
Molecular Formula:C₂₀H₂₃N₅O₄
Molecular Weight:397.434
Hs Code.:

Synonyms:N’-(2-((2,4-dimethoxybenzyl)amino)-8-methylquinazolin-4-yl)-2-hydroxyacetohydrazide

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Chemical Property of N’-(2-((2,4-dimethoxybenzyl)amino)-8-methylquinazolin-4-yl)-2-hydroxyacetohydrazide

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Technology Process of N’-(2-((2,4-dimethoxybenzyl)amino)-8-methylquinazolin-4-yl)-2-hydroxyacetohydrazide

There total 2 articles about N’-(2-((2,4-dimethoxybenzyl)amino)-8-methylquinazolin-4-yl)-2-hydroxyacetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20781-20-8
2,4-Dimethoxybenzylamine

: 1616709-20-6
N’-(2-chloro-8-methylquinazolin-4-yl)-2-hydroxyacetohydrazide

: 1616709-21-7
N’-(2-((2,4-dimethoxybenzyl)amino)-8-methylquinazolin-4-yl)-2-hydroxyacetohydrazide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 100 ℃; for 0.75h;

Reference yield:

: 39576-83-5
2,4,-dichloro-8-methylquinazoline

: 1616709-21-7
N’-(2-((2,4-dimethoxybenzyl)amino)-8-methylquinazolin-4-yl)-2-hydroxyacetohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / 65 °C

2: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 0.75 h / 100 °C

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dimethyl sulfoxide;

Reference yield:

: 1616709-21-7
N’-(2-((2,4-dimethoxybenzyl)amino)-8-methylquinazolin-4-yl)-2-hydroxyacetohydrazide

: 1616709-23-9
2-(chloromethyl)-N-(2,4-dimethoxybenzyl)-7-methyl-[1,2,4]triazolo[1,5-c]quinazolin-5-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,O-Bis(trimethylsilyl)acetamide / 1.5 h / 110 °C

2.1: triethylamine; methanesulfonyl chloride / dichloromethane / 0.67 h / 0 °C

2.2: 2 h / 65 °C

With N,O-Bis(trimethylsilyl)acetamide; methanesulfonyl chloride; triethylamine; In dichloromethane;