Technology Process of C30H35NO5
There total 7 articles about C30H35NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 6 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / Inert atmosphere; Cooling with ice
1.2: 4 h / 0 - 20 °C / Inert atmosphere
2.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 2647.76 Torr
3.1: titanium tetrachloride / dichloromethane / 6 h / -20 °C / Inert atmosphere
4.1: pyridine; hydroxylamine hydrochloride / ethanol / 5 h / Reflux
5.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / ethanol; water / 50 °C / 2250.23 Torr
6.1: triethylamine / dichloromethane / 5.5 h / 0 - 20 °C
With
pyridine; hydrogenchloride; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; titanium tetrachloride; sodium hydride; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; water; mineral oil;
DOI:10.1016/j.bmc.2011.03.064
- Guidance literature:
-
Multi-step reaction with 5 steps
1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 2647.76 Torr
2: titanium tetrachloride / dichloromethane / 6 h / -20 °C / Inert atmosphere
3: pyridine; hydroxylamine hydrochloride / ethanol / 5 h / Reflux
4: hydrogenchloride; palladium 10% on activated carbon; hydrogen / ethanol; water / 50 °C / 2250.23 Torr
5: triethylamine / dichloromethane / 5.5 h / 0 - 20 °C
With
pyridine; hydrogenchloride; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; titanium tetrachloride; triethylamine;
In
ethanol; dichloromethane; water;
DOI:10.1016/j.bmc.2011.03.064