{4-[2-(phenyl(methyl)amino)-4-methylthiazol-5-yl]pyrimidin-2-yl}-N-phenylamine

Base Information

Chemical Name:{4-[2-(phenyl(methyl)amino)-4-methylthiazol-5-yl]pyrimidin-2-yl}-N-phenylamine
CAS No.:930581-48-9
Molecular Formula:C₂₁H₁₉N₅S
Molecular Weight:373.481
Hs Code.:

Synonyms:{4-[2-(phenyl(methyl)amino)-4-methylthiazol-5-yl]pyrimidin-2-yl}-N-phenylamine

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Chemical Property of {4-[2-(phenyl(methyl)amino)-4-methylthiazol-5-yl]pyrimidin-2-yl}-N-phenylamine

Chemical Property:

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Technology Process of {4-[2-(phenyl(methyl)amino)-4-methylthiazol-5-yl]pyrimidin-2-yl}-N-phenylamine

There total 6 articles about {4-[2-(phenyl(methyl)amino)-4-methylthiazol-5-yl]pyrimidin-2-yl}-N-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.6%

: 1333391-55-1
3-dimethylamino-1-[4-methyl-2-(methyl(phenyl)amino)thiazol-5-yl]propenone

: 6685-76-3
phenylguanidinium hydrogencarbonate

: 930581-48-9
{4-[2-(phenyl(methyl)amino)-4-methylthiazol-5-yl]pyrimidin-2-yl}-N-phenylamine

Guidance literature:: With sodium hydroxide; In ethyl methyl ether; at 110 ℃; for 21h; Inert atmosphere;
DOI:10.1002/ardp.201000238

Reference yield:

: 1694-29-7
3-chloropentane-2,4-dione

: 930581-48-9
{4-[2-(phenyl(methyl)amino)-4-methylthiazol-5-yl]pyrimidin-2-yl}-N-phenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / Reflux

2: N,N-dimethyl-formamide / 14 h / 90 °C / Inert atmosphere

3: sodium hydroxide / ethyl methyl ether / 21 h / 110 °C / Inert atmosphere

With sodium hydroxide; In methanol; ethyl methyl ether; N,N-dimethyl-formamide;
DOI:10.1002/ardp.201000238

Reference yield:

: 62-53-3
aniline

: 930581-48-9
{4-[2-(phenyl(methyl)amino)-4-methylthiazol-5-yl]pyrimidin-2-yl}-N-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / 20 - 85 °C

2: sodium hydroxide / ethyl methyl ether / 21 h / 110 °C / Inert atmosphere

With hydrogenchloride; sodium hydroxide; In ethyl methyl ether; water;
DOI:10.1002/ardp.201000238