1-dodecyloxy-4-{4-ethynyl-2,6-bis(hydroxymethyl)-1-phenoxymethyl}benzene

Base Information

Chemical Name:1-dodecyloxy-4-{4-ethynyl-2,6-bis(hydroxymethyl)-1-phenoxymethyl}benzene
CAS No.:1234899-33-2
Molecular Formula:C₂₉H₄₀O₄
Molecular Weight:452.634
Hs Code.:

Synonyms:1-dodecyloxy-4-{4-ethynyl-2,6-bis(hydroxymethyl)-1-phenoxymethyl}benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-dodecyloxy-4-{4-ethynyl-2,6-bis(hydroxymethyl)-1-phenoxymethyl}benzene

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Technology Process of 1-dodecyloxy-4-{4-ethynyl-2,6-bis(hydroxymethyl)-1-phenoxymethyl}benzene

There total 12 articles about 1-dodecyloxy-4-{4-ethynyl-2,6-bis(hydroxymethyl)-1-phenoxymethyl}benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.4%

: 1252783-38-2
C₃₂H₄₆O₅

: 1234899-33-2
1-dodecyloxy-4-{4-ethynyl-2,6-bis(hydroxymethyl)-1-phenoxymethyl}benzene

Guidance literature:: With iso-butanol; sodium hydroxide; at 110 ℃; for 2h;
DOI:10.1021/ma101999k

Reference yield:

: C₃₂H₄₈O₄Si

: 1234899-33-2
1-dodecyloxy-4-{4-ethynyl-2,6-bis(hydroxymethyl)-1-phenoxymethyl}benzene

Guidance literature:: With potassium carbonate; In acetone; at 60 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.polymer.2010.04.030

Reference yield:

: 6296-63-5
4-bromo-2,6-bis(hydroxymethyl)phenol

: 1234899-33-2
1-dodecyloxy-4-{4-ethynyl-2,6-bis(hydroxymethyl)-1-phenoxymethyl}benzene

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / Inert atmosphere

2: copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; triethylamine; triphenylphosphine / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

4: copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; triethylamine; triphenylphosphine / Inert atmosphere

5: potassium carbonate / acetone / 24 h / 60 °C / Inert atmosphere

With pyridine; copper(l) iodide; lithium aluminium tetrahydride; bis(triphenylphosphine)palladium(II) chloride; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1016/j.polymer.2010.04.030