3,5-bis-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-bromomethylbenzene

Base Information

Chemical Name:3,5-bis-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-bromomethylbenzene
CAS No.:271256-09-8
Molecular Formula:C₁₉H₂₉B₂BrO₄
Molecular Weight:422.963
Hs Code.:

Synonyms:3,5-bis-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-bromomethylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-bis-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-bromomethylbenzene

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Technology Process of 3,5-bis-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-bromomethylbenzene

There total 2 articles about 3,5-bis-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-bromomethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

: 1030380-40-5
3,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)toluene

: 271256-09-8
3,5-bis-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-bromomethylbenzene

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 7h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2011.03.025

Reference yield:

: 1611-92-3
3,5-dibromotoluene

: 73183-34-3
bis(pinacol)diborane

: 271256-09-8
3,5-bis-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-bromomethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 4 h / 80 °C / Inert atmosphere

2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 7 h / Inert atmosphere; Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-Bromosuccinimide; potassium acetate; dibenzoyl peroxide; In tetrachloromethane; dimethyl sulfoxide;
DOI:10.1016/j.tet.2011.03.025