(E)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl methyl carbonate

Base Information

Chemical Name:(E)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl methyl carbonate
CAS No.:1108179-34-5
Molecular Formula:C₁₉H₂₄O₇
Molecular Weight:364.395
Hs Code.:

Synonyms:(E)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl methyl carbonate

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Chemical Property of (E)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl methyl carbonate

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Technology Process of (E)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl methyl carbonate

There total 1 articles about (E)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 108182-63-4
(E)-3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hept-5-eno-1,4-furanose

: 79-22-1
methyl chloroformate

: 1108179-34-5
(E)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl methyl carbonate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃;
DOI:10.1039/b813978d

Reference yield:

: 1108179-34-5
(E)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl methyl carbonate

: 63959-88-6
tert-butyl N-(trifluoroacetyl)glycinate

: 5-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-(2S)-(trifluoroacetyl)amino-4-(E)-pentenoic acid tert-butyl ester

: 1108179-42-5
5-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-(2R)-(trifluoroacetyl)amino-4-(E)-pentenoic acid tert-butyl ester

Guidance literature:: tert-butyl N-(trifluoroacetyl)glycinate; With zinc(II) chloride; lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.333333h;

(E)-3-((3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-tetrahydrofuro[2,3-d][1,3]-dioxol-5-yl)-allyl methyl carbonate; With bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine; In tetrahydrofuran; at -78 - 20 ℃; optical yield given as %de;
DOI:10.1039/b813978d