{4-[4-chloro-2-(4-chlorophenylsulfanyl)benzenesulfinyl]phenyl} dimethylamine

Base Information

Chemical Name:{4-[4-chloro-2-(4-chlorophenylsulfanyl)benzenesulfinyl]phenyl} dimethylamine
CAS No.:1044573-06-9
Molecular Formula:C₂₀H₁₇ClFNOS₂
Molecular Weight:405.944
Hs Code.:

Synonyms:{4-[4-chloro-2-(4-chlorophenylsulfanyl)benzenesulfinyl]phenyl} dimethylamine

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Chemical Property of {4-[4-chloro-2-(4-chlorophenylsulfanyl)benzenesulfinyl]phenyl} dimethylamine

Chemical Property:

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Technology Process of {4-[4-chloro-2-(4-chlorophenylsulfanyl)benzenesulfinyl]phenyl} dimethylamine

There total 3 articles about {4-[4-chloro-2-(4-chlorophenylsulfanyl)benzenesulfinyl]phenyl} dimethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 90309-29-8
[4-(4-fluoro-benzenesulfinyl)-phenyl]dimethylamine

: 1213-40-7
S-(4-chlorophenyl)benzene thiosulfonate

: 1044573-06-9
{4-[4-chloro-2-(4-chlorophenylsulfanyl)benzenesulfinyl]phenyl} dimethylamine

Guidance literature:: [4-(4-fluoro-benzenesulfinyl)-phenyl]dimethylamine; With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; In tetrahydrofuran; at -30 ℃; Inert atmosphere;

S-(4-chlorophenyl)benzene thiosulfonate; In tetrahydrofuran; at 25 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol801431z

Reference yield:

: 7152-80-9
4-(dimethylamino)benzenethiocyanate

: 1044573-06-9
{4-[4-chloro-2-(4-chlorophenylsulfanyl)benzenesulfinyl]phenyl} dimethylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / -20 - 25 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; water / -20 °C / Inert atmosphere

3.1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / tetrahydrofuran / -30 °C / Inert atmosphere

3.2: 1 h / 25 °C / Inert atmosphere

With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/chem.201003657

Reference yield:

: 68253-25-8
4-((4-fluorophenyl)thio)-N,N-dimethylaniline

: 1044573-06-9
{4-[4-chloro-2-(4-chlorophenylsulfanyl)benzenesulfinyl]phenyl} dimethylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; water / -20 °C / Inert atmosphere

2.1: 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex / tetrahydrofuran / -30 °C / Inert atmosphere

2.2: 1 h / 25 °C / Inert atmosphere

With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/chem.201003657