(2R,3S)-O,O-DIACETYL-3-DIBENZYLAMINO-4-PHENYLBUTANE-1,2-DIOL

Base Information

Chemical Name:(2R,3S)-O,O-DIACETYL-3-DIBENZYLAMINO-4-PHENYLBUTANE-1,2-DIOL
CAS No.:871948-89-9
Molecular Formula:C₂₈H₃₁NO₄
Molecular Weight:445.558
Hs Code.:
Mol file:871948-89-9.mol

Synonyms:1,2-Butanediol,3-[bis(phenylmethyl)amino]-4-phenyl-, diacetate (ester), (2R,3S)- (9CI)

Suppliers and Price of (2R,3S)-O,O-DIACETYL-3-DIBENZYLAMINO-4-PHENYLBUTANE-1,2-DIOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(2R,3S)-O,O-DIACETYL-3-DIBENZYLAMINO-4-PHENYLBUTANE-1,2-DIOL 95.00%
5MG
$ 502.94

Total 8 raw suppliers

Chemical Property of (2R,3S)-O,O-DIACETYL-3-DIBENZYLAMINO-4-PHENYLBUTANE-1,2-DIOL

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:567.513°C at 760 mmHg
Flash Point:297.021°C
PSA：55.84000
Density:1.14g/cm³
LogP:4.79490

Purity/Quality:

99% ^*data from raw suppliers

(2R,3S)-O,O-DIACETYL-3-DIBENZYLAMINO-4-PHENYLBUTANE-1,2-DIOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2R,3S)-O,O-DIACETYL-3-DIBENZYLAMINO-4-PHENYLBUTANE-1,2-DIOL

There total 2 articles about (2R,3S)-O,O-DIACETYL-3-DIBENZYLAMINO-4-PHENYLBUTANE-1,2-DIOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 64-19-7,77671-22-8
acetic acid

: 127943-39-9
(1R)-[1'(S)-(dibenzylamino)-2'-phenylethyl]oxirane

: 871948-89-9
(2R,3S)-O,O-diacetyl-3-dibenzylamino-4-phenylbutane-1,2-diol

Guidance literature:: With boron trifluoride diethyl etherate; In acetonitrile; at 80 ℃; for 12h;
DOI:10.1021/jo0514873

Reference yield:

: 64-19-7,77671-22-8
acetic acid

: 127943-39-9
(1R)-[1'(S)-(dibenzylamino)-2'-phenylethyl]oxirane

: 871948-89-9
(2R,3S)-O,O-diacetyl-3-dibenzylamino-4-phenylbutane-1,2-diol

: 4-phenyl-3-aminobutane-1,2-diol

Guidance literature:: acetic acid; (1R)-[1'(S)-(dibenzylamino)-2'-phenylethyl]oxirane; With boron trifluoride diethyl etherate; In acetonitrile; at 80 ℃; for 12h;

With sodium hydrogencarbonate; In acetonitrile; at 20 ℃; for 0.0833333h;
DOI:10.1021/jo0514873