C₁₀H₁₄O₃

Base Information

Chemical Name:C₁₀H₁₄O₃
CAS No.:1270038-99-7
Molecular Formula:C₁₀H₁₄O₃
Molecular Weight:182.219
Hs Code.:

C<sub>10</sub>H<sub>14</sub>O<sub>3</sub>

Synonyms:C₁₀H₁₄O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₁₄O₃

Chemical Property:

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Technology Process of C₁₀H₁₄O₃

There total 3 articles about C₁₀H₁₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 96-49-1
[1,3]-dioxolan-2-one

: 2785-78-6
3,6-Dimethylcatechol

: 1270038-99-7
C₁₀H₁₄O₃

Guidance literature:: With tetra-(n-butyl)ammonium iodide; at 150 ℃; for 12h; Inert atmosphere;
DOI:10.3987/COM-10-S(E)22

Reference yield:

: 95-87-4
2,5-Dimethylphenol

: 1270038-99-7
C₁₀H₁₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium chloride; triethylamine / acetonitrile / 0.25 h / 20 °C / Reflux; Inert atmosphere

1.2: 2.5 h / 100 °C

2.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 0.33 h / 0 - 20 °C / Inert atmosphere

3.1: tetra-(n-butyl)ammonium iodide / 12 h / 150 °C / Inert atmosphere

With dihydrogen peroxide; tetra-(n-butyl)ammonium iodide; triethylamine; sodium hydroxide; magnesium chloride; In tetrahydrofuran; water; acetonitrile; 1.1: |Dakin Phenol Oxidation;
DOI:10.3987/COM-10-S(E)22

Reference yield:

: 1666-04-2
2-hydroxy-3,6-dimethylbenzaldehyde

: 1270038-99-7
C₁₀H₁₄O₃

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 0.33 h / 0 - 20 °C / Inert atmosphere

2: tetra-(n-butyl)ammonium iodide / 12 h / 150 °C / Inert atmosphere

With dihydrogen peroxide; tetra-(n-butyl)ammonium iodide; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.3987/COM-10-S(E)22