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High quality Ethylene Carbonate supplier in China
Cas No: 96-49-1
No Data 1 Metric Ton 6000 Metric Ton/Year Simagchem Corporation Contact Supplier
High purity Ethylene Carbonate
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USD $ 1.0-1.5 / Kilogram 1 Kilogram 2000 Metric Ton/Year Xiamen BaiFuchem Co.,Ltd Contact Supplier
High quality Ethylene Carbonate for hot sale
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Ethylene Carbonate(EC)
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Ethylene carbonate
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High purity 96-49-1 Ethylene carbonate
Cas No: 96-49-1
USD $ 100.0-500.0 / Gram 1 Gram 99999 Gram/Year Hangzhou Dingyan Chem Co., Ltd Contact Supplier
Ethylene carbonate 96-49-1 China Factory Ethylene carbonate CAS 96-49-1
Cas No: 96-49-1
USD $ 100.0-110.0 / Kilogram 1 Kilogram 500 Metric Ton/Month Hebei Yingong New Material Technology Co.,Ltd . Contact Supplier
Factory price Cosmetic ETHYLENE CARBONATE 96-49-1 Manufacturer
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USD $ 0.1-0.1 / Gram 1 Gram 100 Metric Ton/Year Xi'an Xszo Chem Co., Ltd. Contact Supplier
Ethylene carbonate
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No Data 1 Gram 20 Metric Ton/Week Henan Allgreen Chemical Co.,Ltd Contact Supplier
Factory Supply Ethylene carbonate
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96-49-1 Usage

Uses

Ethylene carbonate is an ester of ethylene glycol and carbonic acid. Ethylene carbonate is used as a polar solvent with a molecular dipole moment of 4.9 D, only 0.1 D lower than that of propylene carb onate. It can be used as a high permittivity component of electrolytes in lithium batteries.

Chemical Properties

colourless crystals

Purification Methods

Dry 1,3-dioxolan-2-one over P2O5, then fractionally distil it at low or atmospheric pressure. Recrystallise it from dry Et2O (plates, m 36.5o, 38.5-40o was also reported). It is soluble in H2O. [Beilstein 19 II 135,19 III/IV 1556, 19/4 V 6.]
InChI:InChI=1/C3H4O3/c4-3-5-1-2-6-3/h1-2H2

96-49-1 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A15735)  Ethylene carbonate, 99%    96-49-1 500g 144.0CNY Detail
Alfa Aesar (A15735)  Ethylene carbonate, 99%    96-49-1 2500g 530.0CNY Detail
Alfa Aesar (A15735)  Ethylene carbonate, 99%    96-49-1 10000g 1962.0CNY Detail
Sigma-Aldrich (676802)  Ethylenecarbonate  anhydrous, 99% 96-49-1 676802-1L 1,776.06CNY Detail
Sigma-Aldrich (676802)  Ethylenecarbonate  anhydrous, 99% 96-49-1 676802-6X1L 7,289.10CNY Detail
Aldrich (E26258)  Ethylenecarbonate  98% 96-49-1 E26258-100G 216.45CNY Detail
Aldrich (E26258)  Ethylenecarbonate  98% 96-49-1 E26258-500G 279.63CNY Detail
Aldrich (E26258)  Ethylenecarbonate  98% 96-49-1 E26258-3KG 1,396.98CNY Detail

96-49-1SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 17, 2017

Revision Date: Aug 17, 2017

1.Identification

1.1 GHS Product identifier

Product name Ethylene carbonate

1.2 Other means of identification

Product number -
Other names 1,3-Dioxolan-2-one

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Adhesives and sealant chemicals,Intermediates
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:96-49-1 SDS

96-49-1Synthetic route

oxirane
75-21-8

oxirane

carbon dioxide
124-38-9

carbon dioxide

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With 3-(2-hydroxylethyl)-1-(3-aminopropyl)imidazolium bromide grafted onto divinylbenzene polymer (PDVB-HEIMBr) at 140℃; under 15001.5 Torr; for 3h; Autoclave;100%
With bis[(1R,2R)-N,N'-bis(3,5-di-tert-butyl-salicylidene)cyclohexane-1,2-diaminoaluminium(III)]oxide; tetrabutylammomium bromide at 26℃; under 2280.15 Torr; for 24h;100%
With choline chloride; zinc dibromide at 110℃; under 11251.1 Torr; for 1h; Autoclave; neat (no solvent);100%
carbon dioxide
124-38-9

carbon dioxide

ethylene glycol
107-21-1

ethylene glycol

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With 2-Cyanopyridine; cerium(IV) oxide at 129.84℃; under 37503.8 Torr; for 1h; Autoclave;99%
With 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate at 70℃; under 7500.75 Torr; for 18h; Reagent/catalyst; Solvent; Pressure; Autoclave;74%
With 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,2-dibromomethane at 70℃; under 7500.75 Torr; for 18h; Reagent/catalyst; Autoclave; Ionic liquid;74%
oxirane
75-21-8

oxirane

piperazine-1-carboxylic acid
10430-90-7

piperazine-1-carboxylic acid

A

piperazine
110-85-0

piperazine

B

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With zinc dibromide at 160℃; for 8.5h;A 97.7%
B 94.9%
ethylene glycol
107-21-1

ethylene glycol

urea
57-13-6

urea

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With Zn6Al2(OH)16CO3·6H2O at 130℃; under 22.5023 Torr; for 3h; Reagent/catalyst; Time;96%
With zinc(II) chloride at 160℃; under 112.511 Torr; for 3h; Reagent/catalyst; Temperature; Pressure; Ionic liquid;92.7%
With 1-hexadecyl-3-methylimidazolium chloride; zinc(II) chloride In neat (no solvent) at 140℃; under 112.511 Torr; for 3h; Reagent/catalyst; Temperature; Pressure; Green chemistry;92.2%
oxirane
75-21-8

oxirane

N-β-aminoethylcarbamic acid
109-58-0

N-β-aminoethylcarbamic acid

A

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

B

ethylenediamine
107-15-3

ethylenediamine

Conditions
ConditionsYield
With zinc(II) oxide at 100℃; for 0.5h;A 92.6%
B 95.2%
ethylene glycol
107-21-1

ethylene glycol

Diethyl carbonate
105-58-8

Diethyl carbonate

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
MCM-41-TBD; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine for 15h; Heating;95%
With potassium carbonate at 105℃; Entfernen des entstehenden Aethanols;
tiveTMNano*MgO*Plus*(NAP-MgO,*Aerogel*prepared) at 125℃; for 1h;
Tetramethylammonium hydrogen carbonate
58345-96-3

Tetramethylammonium hydrogen carbonate

2-bromoethanol
540-51-2

2-bromoethanol

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.166667h;95%
carbon dioxide
124-38-9

carbon dioxide

N,N-dimethylformamide ethylene acetal
19449-26-4

N,N-dimethylformamide ethylene acetal

A

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

B

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

Conditions
ConditionsYield
at 110℃; under 37503 Torr; for 15h;A 95%
B n/a
ethylene glycol
107-21-1

ethylene glycol

carbonic acid dimethyl ester
616-38-6

carbonic acid dimethyl ester

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With dicobalt octacarbonyl at 180℃; for 1h;95%
With 1,1,1-trioctyl-1-methylphosphonium methylcarbonate at 90℃; for 4h;86%
ytterbium(III) triflate In 1,2-dichloro-ethane for 8h; Heating;41%
Tetramethylammonium hydrogen carbonate
58345-96-3

Tetramethylammonium hydrogen carbonate

2-chloro-ethanol
107-07-3

2-chloro-ethanol

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
In acetonitrile at 20℃; for 0.75h;94%
potassium carbonate
584-08-7

potassium carbonate

ethylene dibromide
106-93-4

ethylene dibromide

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
18-crown-6 ether; bis(tributyltin)sulfide In acetonitrile at 80℃; for 10h;93%
18-crown-6 ether; bis(tributyltin)sulfide In acetonitrile at 80℃; for 10h; various catalysts, and catalytic systems; further alkyl bromides;93%
Iodoethanol
624-76-0

Iodoethanol

carbon dioxide
124-38-9

carbon dioxide

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With caesium carbonate In N,N-dimethyl-formamide at 40℃; under 760.051 Torr; for 15h; Inert atmosphere; Glovebox; Green chemistry;92%
bis(phenyl) carbonate
102-09-0

bis(phenyl) carbonate

ethylene glycol
107-21-1

ethylene glycol

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In 2-methyltetrahydrofuran at 30℃; for 2h;91%
Ethyl trichloroacetate
515-84-4

Ethyl trichloroacetate

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
In potassium carbonate; ethylene glycol90%
With dmap In ethylene glycol
carbon monoxide
201230-82-2

carbon monoxide

ethylene glycol
107-21-1

ethylene glycol

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With N-chloro-succinimide; (neocuproine)Pd(OAc)2; sodium acetate In acetonitrile at 55℃; under 760.051 Torr; for 24h; Molecular sieve;89%
With air; potassium iodide; palladium(II) iodide In ISOPROPYLAMIDE at 100℃; under 15201 Torr; for 15h; Autoclave;84%
With oxygen; potassium iodide; palladium(II) iodide In N,N-dimethyl acetamide at 100℃; under 15201 Torr; for 15h;84%
oxirane
75-21-8

oxirane

carbon monoxide
201230-82-2

carbon monoxide

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With 1-carboxypropyl-imidazolium bromide at 120℃; under 11251.1 Torr; for 2h;87.33%
2,2'-dipyridyl carbonate
1659-31-0

2,2'-dipyridyl carbonate

ethylene glycol
107-21-1

ethylene glycol

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
In toluene at 110℃; for 1h;85%
carbon dioxide
124-38-9

carbon dioxide

2-bromoethanol
540-51-2

2-bromoethanol

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
Stage #1: carbon dioxide With potassium carbonate In N,N-dimethyl-formamide at 30℃; under 760.051 Torr; for 4h;
Stage #2: 2-bromoethanol In N,N-dimethyl-formamide at 30℃; for 20h;
81%
With caesium carbonate In N,N-dimethyl-formamide at 40℃; under 760.051 Torr; for 15h; Inert atmosphere; Glovebox; Green chemistry;75%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In water; acetone at 100℃; under 4654.46 Torr; for 0.166667h; Flow reactor;
phosgene
75-44-5

phosgene

2,2-dibutyl[1,3,2]dioxastannolane
3590-59-8

2,2-dibutyl[1,3,2]dioxastannolane

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
for 0.5h;78%
oxirane
75-21-8

oxirane

ethanol
64-17-5

ethanol

carbon dioxide
124-38-9

carbon dioxide

A

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

B

2-ethoxy-ethanol
110-80-5

2-ethoxy-ethanol

C

ethylene glycol
107-21-1

ethylene glycol

Conditions
ConditionsYield
With lanthanum(III) oxide; potassium iodide at 149.84℃; under 22502.3 Torr; for 3h;A 77.3%
B 14.1%
C 6.8%
oxirane
75-21-8

oxirane

ethanol
64-17-5

ethanol

carbon dioxide
124-38-9

carbon dioxide

A

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

B

ethylene glycol
107-21-1

ethylene glycol

Conditions
ConditionsYield
With potassium iodide; magnesium carbonate at 149.84℃; under 22502.3 Torr; for 3h;A 75.7%
B 6.7%
oxalyl dichloride
79-37-8

oxalyl dichloride

ethylene glycol
107-21-1

ethylene glycol

A

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

B

1,4-dioxane-2,3-dione
3524-70-7

1,4-dioxane-2,3-dione

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 0℃; for 0.333333h;A n/a
B 72%
With triethylamine 1.) THF, 15 min, 0 deg C; 2.) 200-300 deg C, 10.5 hrs; Yield given;A 1.9%
B n/a
carbon dioxide
124-38-9

carbon dioxide

2-chloro-ethanol
107-07-3

2-chloro-ethanol

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
Stage #1: carbon dioxide With potassium carbonate In N,N-dimethyl-formamide at 30℃; under 760.051 Torr; for 4h;
Stage #2: 2-chloro-ethanol In N,N-dimethyl-formamide at 30℃; for 20h;
72%
With potassium carbonate In PEG-400 at 50℃; under 15001.5 Torr; for 3h; Autoclave;> 99 %Chromat.
With ethyl(8-diisopropylamino-3,6-dioxaoctyl)dimethylammonium bis{(trifluoromethyl)sulfonyl}azanide at 25℃; under 7500.75 Torr; for 48h; Autoclave; Green chemistry;
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dimethyl sulfoxide at 20℃; for 0.333333h; Mechanism; Solvent;
With tetrabutylammomium bromide; silica gel; potassium carbonate at 110℃; under 7600.51 Torr; for 2h; Catalytic behavior; Reagent/catalyst; Temperature; Pressure; Autoclave;
4-(trifluoromethoxy)benzonitrile
332-25-2

4-(trifluoromethoxy)benzonitrile

ethylene glycol
107-21-1

ethylene glycol

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With 3,7-di([1,1′-biphenyl]-4-yl)-10-(naphthalen-1-yl)-10H-phenoxazine; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 24h; Reagent/catalyst; Inert atmosphere; Irradiation; Sealed tube;70%
oxirane
75-21-8

oxirane

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
With carbon dioxide; Ni(P(C6H11-cyclo)3)2 In toluene at 100℃; under 3677.5 - 4413.05 Torr; for 24h; Product distribution; yield by different catalysts;62%
With carbon dioxide
oxirane
75-21-8

oxirane

CO2

CO2

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

Conditions
ConditionsYield
Ni(P(C6H11-cyclo)3)2 In toluene at 100℃; under 3677.5 - 4413.05 Torr; for 24h;62%
1,3-DIOXOLANE
646-06-0

1,3-DIOXOLANE

A

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

B

ethylene glycol monoformate
628-35-3

ethylene glycol monoformate

Conditions
ConditionsYield
With oxygen; CoCl2 In 1,2-dimethoxyethane at 60℃; for 24h;A 10%
B 61%
Bromoform
75-25-2

Bromoform

2-(hexyloxy)-1,3-dioxolane
83498-70-8

2-(hexyloxy)-1,3-dioxolane

A

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

B

1-bromo-hexane
111-25-1

1-bromo-hexane

C

formic acid-(2-bromo-ethyl ester)
6065-67-4

formic acid-(2-bromo-ethyl ester)

D

hexanal
66-25-1

hexanal

E

2-bromoethyl hexyl carbonate

2-bromoethyl hexyl carbonate

F

1,2-dibromomethane
74-95-3

1,2-dibromomethane

Conditions
ConditionsYield
dibenzoyl peroxide at 100℃; for 2h; Rate constant; Product distribution; other temperature;A n/a
B n/a
C n/a
D n/a
E 60%
F n/a
Bis<1,2-ethanediyl> orthocarbonate
24471-99-6

Bis<1,2-ethanediyl> orthocarbonate

A

[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

B

Carbonic acid bis-(2-hydroxy-ethyl) ester

Carbonic acid bis-(2-hydroxy-ethyl) ester

Conditions
ConditionsYield
With hydrogenchloride In water for 0.166667h; Product distribution; Ambient temperature; study of the acid catalyzed hydrolysis reaction of various spiroorthocarbonates, mechanism is discussed, mechanism is discussed;A 56%
B 24%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

propan-1-ol-3-amine
156-87-6

propan-1-ol-3-amine

(3-hydroxy-propyl)-carbamic acid-(2-hydroxy-ethyl ester)
69506-93-0

(3-hydroxy-propyl)-carbamic acid-(2-hydroxy-ethyl ester)

Conditions
ConditionsYield
1) 50-55 deg C, 1 h; 2) r.t., overnight;100%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

2-hydroxyethyl carbamate
5395-01-7

2-hydroxyethyl carbamate

Conditions
ConditionsYield
With ammonia In water 1.) 0 deg C, 4 h, 2.) 25 deg C, overnight;100%
With ammonia at 20℃; under 600.048 Torr; for 1h; Addition; solid-gas reaction; ring cleavage;92%
With ammonia; water
With ammonia; water
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

4-Fluorophenol
371-41-5

4-Fluorophenol

2-(4'-fluorophenoxy)ethanol
2924-66-5

2-(4'-fluorophenoxy)ethanol

Conditions
ConditionsYield
With potassium fluoride at 160℃;100%
With potassium carbonate In N,N-dimethyl-formamide at 110℃; for 18h; Inert atmosphere;82%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

2,6-Dichlorophenol
87-65-0

2,6-Dichlorophenol

2-(2,6-dichlorophenoxy)ethanol
42001-44-5

2-(2,6-dichlorophenoxy)ethanol

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide for 2h; Heating;100%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

2-methoxy-4-nitrophenol
3251-56-7

2-methoxy-4-nitrophenol

2-(2-methoxy-4-nitrophenoxy)ethanol

2-(2-methoxy-4-nitrophenoxy)ethanol

Conditions
ConditionsYield
With tetra-(n-butyl)ammonium iodide at 160℃; for 2h;100%
With tetra-(n-butyl)ammonium iodide; magnesium sulfate In chloroform
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

2-Anilinoethanol
122-98-5

2-Anilinoethanol

N-phenyl-2-oxazolidinone
703-56-0

N-phenyl-2-oxazolidinone

Conditions
ConditionsYield
With 1-n-butyl-3-methylimidazolim bromide; 3-butyl-1-methylimidazolium acetate at 140℃; for 9h;99%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

phenol
108-95-2

phenol

2-Phenoxyethanol
122-99-6

2-Phenoxyethanol

Conditions
ConditionsYield
With potassium fluoride99%
With potassium iodide97.7%
With tetrabutyl ammonium fluoride In N,N-dimethyl-formamide at 170℃; for 0.583333h; Inert atmosphere; Schlenk technique;94%
With tetraethylammonium iodide
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

ethylene glycol
107-21-1

ethylene glycol

Conditions
ConditionsYield
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate; hydrogen In tetrahydrofuran at 140℃; under 38002.6 Torr; for 0.5h; Time; Pressure; Autoclave;99%
In water at 250℃; for 2h; Temperature; Sealed tube; Inert atmosphere;99%
With potassium tert-butylate; hydrogen; C16H18BrCoINO2 In dibutyl ether at 160℃; under 45004.5 Torr; for 20h; Sealed tube; Autoclave;92%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

meta-hydroxyacetanilide
621-42-1

meta-hydroxyacetanilide

acetic acid-[3-(2-hydroxy-ethoxy)-anilide]

acetic acid-[3-(2-hydroxy-ethoxy)-anilide]

Conditions
ConditionsYield
In methanol; ethyl acetate; toluene99%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

ethanol
64-17-5

ethanol

Diethyl carbonate
105-58-8

Diethyl carbonate

Conditions
ConditionsYield
With Zn6Al2(OH)16NO3·nΗ2O at 83℃; for 6h; Reagent/catalyst; Time;99%
at 69.84℃; for 6h; Catalytic behavior; Reagent/catalyst;78.1%
With carbon dioxide at 160℃; under 4500.45 Torr; for 4h; Autoclave;40.5%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
25015-63-8

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

1,2-bis((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)oxy)ethane
97174-38-4

1,2-bis((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)oxy)ethane

Conditions
ConditionsYield
With manganese(II) triflate bis-acetonitrile solvate; potassium tert-butylate In benzene-d6 at 20℃; for 3h; Reagent/catalyst; Inert atmosphere; Glovebox;99%
With tris(bis(trimethylsilyl)amido)lanthanum(III) at 20℃; for 6h; Reagent/catalyst; Inert atmosphere;99 %Spectr.
With C42H50Mg2N4 for 6h; Catalytic behavior;99 %Spectr.
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

1,3-bis(methylamino)propane
111-33-1

1,3-bis(methylamino)propane

C11H22N2O6

C11H22N2O6

Conditions
ConditionsYield
at 80℃; for 47h; Inert atmosphere;99%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

2,4-bisbenzyloxy-N-butyl-5-(5-hydroxy-1,3-dihydroisoindole-2-carbonyl)-N-methylbenzamide
1126832-47-0

2,4-bisbenzyloxy-N-butyl-5-(5-hydroxy-1,3-dihydroisoindole-2-carbonyl)-N-methylbenzamide

2,4-bisbenzyloxy-N-butyl-5-[5-(2-hydroxyethoxy)-1,3-dihydroisoindole-2-carbonyl]-2,4-dihydroxy-N-methylbenzamide
1126832-54-9

2,4-bisbenzyloxy-N-butyl-5-[5-(2-hydroxyethoxy)-1,3-dihydroisoindole-2-carbonyl]-2,4-dihydroxy-N-methylbenzamide

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 80℃; for 16h;98.9%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

4-fluoro-1,3-dioxolane-2-one
114435-02-8

4-fluoro-1,3-dioxolane-2-one

Conditions
ConditionsYield
With N-fluorobis(benzenesulfon)imide at 120℃; for 0.5h; Reagent/catalyst; Sealed tube;98.2%
With fluorine at 5℃; Electrolysis;94%
With fluorine at 50℃;70%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

N-butylamine
109-73-9

N-butylamine

2-hydroxyethyl N-butylcarbamate
13105-54-9

2-hydroxyethyl N-butylcarbamate

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; for 24h; Inert atmosphere;98%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

3-nitro-aniline
99-09-2

3-nitro-aniline

3-(3-nitrophenyl)oxazolidin-2-one
5198-51-6

3-(3-nitrophenyl)oxazolidin-2-one

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane at 100℃; for 5h; Inert atmosphere;98%
With triethylamine; adenine In neat (no solvent) at 110℃; for 18h;95%
With lithium chloride at 176℃; for 8h;
With acetate-based butylimidazolium ionic liquid immobilized silica-coated magnetic nanoparticles In neat (no solvent) at 120℃; for 12h; Green chemistry;
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

N,N'-bis(trimethylsilyl)hydrazine
692-56-8

N,N'-bis(trimethylsilyl)hydrazine

methylamine
74-89-5

methylamine

Methyl-carbamic acid 2-trimethylsilanyloxy-ethyl ester
79967-00-3

Methyl-carbamic acid 2-trimethylsilanyloxy-ethyl ester

Conditions
ConditionsYield
98%
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

4-nitro-phenol
100-02-7

4-nitro-phenol

2-(4-nitrophenoxy)ethanol
16365-27-8

2-(4-nitrophenoxy)ethanol

Conditions
ConditionsYield
With tetrabutyl ammonium fluoride In N,N-dimethyl-formamide at 170℃; for 21h; Inert atmosphere; Schlenk technique;98%
With potassium carbonate In N,N-dimethyl-formamide at 110℃; for 16h; Inert atmosphere;89%
With tetraethylammonium iodide at 150℃;
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

4-bromo-3-methylphenol
14472-14-1

4-bromo-3-methylphenol

2-(4-bromo-3-methylphenoxy)ethanol
26738-92-1

2-(4-bromo-3-methylphenoxy)ethanol

Conditions
ConditionsYield
With potassium carbonate In toluene at 115℃; for 24h; Product distribution / selectivity;98%
With potassium carbonate In toluene at 115℃; for 24h; Inert atmosphere;98%
With potassium carbonate In N,N-dimethyl-formamide86%

96-49-1Downstream Products

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