tert-butyldiphenyl((17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraenyloxy)silane

Base Information

Chemical Name:tert-butyldiphenyl((17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraenyloxy)silane
CAS No.:1260225-98-6
Molecular Formula:C₅₄H₈₀O₃SSi
Molecular Weight:837.379
Hs Code.:

Synonyms:tert-butyldiphenyl((17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraenyloxy)silane

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Chemical Property of tert-butyldiphenyl((17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraenyloxy)silane

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Technology Process of tert-butyldiphenyl((17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraenyloxy)silane

There total 6 articles about tert-butyldiphenyl((17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraenyloxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 56401-77-5
(5Z,8Z,11Z,14Z)-icosa-5,8,11,14-tetraenyl-4-methylbenzenesulfonate

: 1260225-80-6
tert-butyldiphenyl(12-(phenylsulfonyl)dodecyloxy)silane

: 1260225-98-6
tert-butyldiphenyl((17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraenyloxy)silane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12.5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.09.139

Reference yield:

: 506-32-1,236743-58-1
all cis 5,8,11,14-eicosatetraenoic acid

: 1260225-98-6
tert-butyldiphenyl((17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraenyloxy)silane

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

1.2: 1 h

2.1: pyridine / 4 h / 0 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / -78 - 20 °C / Inert atmosphere

3.2: -10 °C

With lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; pyridine; hexane;

Reference yield:

: 227186-15-4
[(12-bromododecyl)oxy](tert-butyl)diphenylsilane

: 1260225-98-6
tert-butyldiphenyl((17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraenyloxy)silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 3 h / 70 °C / Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.2: -10 °C

With n-butyllithium; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;