(17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraen-1-ol

Base Information

Chemical Name:(17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraen-1-ol
CAS No.:1260226-00-3
Molecular Formula:C₃₈H₆₂O₃S
Molecular Weight:598.974
Hs Code.:

Synonyms:(17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraen-1-ol

Suppliers and Price of (17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraen-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraen-1-ol

Chemical Property:

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Technology Process of (17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraen-1-ol

There total 7 articles about (17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1260225-98-6
tert-butyldiphenyl((17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraenyloxy)silane

: 1260226-00-3
(17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraen-1-ol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2010.09.139

Reference yield:

: 506-32-1,236743-58-1
all cis 5,8,11,14-eicosatetraenoic acid

: 1260226-00-3
(17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraen-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

1.2: 1 h

2.1: pyridine / 4 h / 0 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / -78 - 20 °C / Inert atmosphere

3.2: -10 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h

With lithium aluminium tetrahydride; n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran; pyridine; hexane;

Reference yield:

: 227186-15-4
[(12-bromododecyl)oxy](tert-butyl)diphenylsilane

: 1260226-00-3
(17Z,20Z,23Z,26Z)-12-(phenylsulfonyl)dotriaconta-17,20,23,26-tetraen-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide / 3 h / 70 °C / Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.2: -10 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h

With n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;