6-(4-Chlorophenylthiomethyl)-2-(4-morpholinyl)-1,4,3-oxathiazin-4,4-dioxid

Base Information

Chemical Name:6-(4-Chlorophenylthiomethyl)-2-(4-morpholinyl)-1,4,3-oxathiazin-4,4-dioxid
CAS No.:117239-21-1
Molecular Formula:C₁₄H₁₅ClN₂O₄S₂
Molecular Weight:374.869
Hs Code.:

Synonyms:6-(4-Chlorophenylthiomethyl)-2-(4-morpholinyl)-1,4,3-oxathiazin-4,4-dioxid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(4-Chlorophenylthiomethyl)-2-(4-morpholinyl)-1,4,3-oxathiazin-4,4-dioxid

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Technology Process of 6-(4-Chlorophenylthiomethyl)-2-(4-morpholinyl)-1,4,3-oxathiazin-4,4-dioxid

There total 3 articles about 6-(4-Chlorophenylthiomethyl)-2-(4-morpholinyl)-1,4,3-oxathiazin-4,4-dioxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 117239-12-0
6-(Chloromethyl)-2-(4-morpholinyl)-1,4,3-oxathiazin-4,4-dioxid

: 106-54-7
p-Chlorothiophenol

: 117239-21-1
6-(4-Chlorophenylthiomethyl)-2-(4-morpholinyl)-1,4,3-oxathiazin-4,4-dioxid

Guidance literature:: With triethylamine; In ethanol; 1.) room temp., 1 h; 2.) reflux, 3 h;
DOI:10.1055/s-1988-27623

Reference yield:

: 1530-89-8
N-cyanomorpholine

: 117239-21-1
6-(4-Chlorophenylthiomethyl)-2-(4-morpholinyl)-1,4,3-oxathiazin-4,4-dioxid

Guidance literature:: Multi-step reaction with 3 steps

1: 1,2-dimethoxy-ethane / 1 h / Ambient temperature

2: 1,2-dimethoxy-ethane / 3 h / 80 °C

3: 85 percent / Et₃N / ethanol / 1.) room temp., 1 h; 2.) reflux, 3 h

With triethylamine; In 1,2-dimethoxyethane; ethanol;
DOI:10.1055/s-1988-27623

Reference yield:

: (2-Morpholin-4-yl-4,4-dioxo-4H-4λ⁶-[1,4,3]oxathiazin-6-yl)-methanesulfonyl chloride

: 117239-21-1
6-(4-Chlorophenylthiomethyl)-2-(4-morpholinyl)-1,4,3-oxathiazin-4,4-dioxid

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2-dimethoxy-ethane / 3 h / 80 °C

2: 85 percent / Et₃N / ethanol / 1.) room temp., 1 h; 2.) reflux, 3 h

With triethylamine; In 1,2-dimethoxyethane; ethanol;
DOI:10.1055/s-1988-27623