Technology Process of C31H42FN3O8Si
There total 21 articles about C31H42FN3O8Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,3-dimethylbarbituric acid;
tetrakis(triphenylphosphine) palladium(0);
In
dichloromethane; ethyl acetate;
at 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / chloroform / 16 h / 0 - 20 °C / Inert atmosphere
2: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium(0) / dichloromethane; ethyl acetate / 20 °C / Inert atmosphere
With
1,3-dimethylbarbituric acid; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine;
tetrakis(triphenylphosphine) palladium(0);
In
dichloromethane; chloroform; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 0 - 20 °C
2: 1-amino-3-(dimethylamino)propane / tetrahydrofuran / 0 - 20 °C
3: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / chloroform / 16 h / 0 - 20 °C / Inert atmosphere
4: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium(0) / dichloromethane; ethyl acetate / 20 °C / Inert atmosphere
With
1,3-dimethylbarbituric acid; 1-amino-3-(dimethylamino)propane; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; dichloromethane; chloroform; ethyl acetate;