[4-(1-pyrrolidinylmethyl)-3-(trifluoromethyl)phenyl]carbamic acid phenyl ester

Base Information

• Chemical Name: [4-(1-pyrrolidinylmethyl)-3-(trifluoromethyl)phenyl]carbamic acid phenyl ester
• CAS No.: 882408-06-2
• Molecular Formula: C₁₉H₁₉F₃N₂O₂
• Molecular Weight: 364.367

Synonyms:[4-(1-pyrrolidinylmethyl)-3-(trifluoromethyl)phenyl]carbamic acid phenyl ester

Chemical Property of [4-(1-pyrrolidinylmethyl)-3-(trifluoromethyl)phenyl]carbamic acid phenyl ester

Chemical Property:

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Technology Process of [4-(1-pyrrolidinylmethyl)-3-(trifluoromethyl)phenyl]carbamic acid phenyl ester

There total 1 articles about [4-(1-pyrrolidinylmethyl)-3-(trifluoromethyl)phenyl]carbamic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-pyrrolidin-1-ylmethyl-3-trifluoromethyl-phenylamine (882408-16-4) + phenyl chloroformate (1885-14-9) → [4-(1-pyrrolidinylmethyl)-3-(trifluoromethyl)phenyl]carbamic acid phenyl ester (882408-06-2)

Guidance literature:

With pyridine; In tetrahydrofuran; at -70 ℃; for 1h; Product distribution / selectivity;

Reference yield:

6-amino-4-(1,2,3,4-tetrahydro-quinolin-6-yloxy)-pyrimidine (882407-94-5) + [4-(1-pyrrolidinylmethyl)-3-(trifluoromethyl)phenyl]carbamic acid phenyl ester (882408-06-2) → 6-(6-amino-pyrimidin-4-yloxy)-3,4-dihydro-2H-quinoline-1-carboxylic acid (4-pyrrolidin-1-ylmethyl-3-trifluoromethyl-phenyl)-amide (882405-67-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 60 ℃; for 3h;

upstream raw materials:

4-pyrrolidin-1-ylmethyl-3-trifluoromethyl-phenylamine

phenyl chloroformate

Downstream raw materials:

6-(6-amino-pyrimidin-4-yloxy)-3,4-dihydro-2H-quinoline-1-carboxylic acid (4-pyrrolidin-1-ylmethyl-3-trifluoromethyl-phenyl)-amide

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