Technology Process of C37H45NO7
There total 9 articles about C37H45NO7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
N,N-dimethyl-formamide;
With
trichlorophosphate;
for 0.75h;
Cooling with ice;
C36H45NO6;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 0.25h;
Microwave irradiation;
Sealed tube;
With
water; sodium acetate;
In
N,N-dimethyl-formamide;
Heating;
DOI:10.1021/ol1027877
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / dimethyl sulfoxide / 1.5 h / 55 °C
2.1: ammonium acetate; acetic acid / 6 h / 100 °C
3.1: lithium borohydride; chloro-trimethyl-silane / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere
4.1: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
4.2: 8 h / 60 °C / Inert atmosphere
5.1: trichlorophosphate / 0.75 h / Cooling with ice
5.2: 0.25 h / 100 °C / Microwave irradiation; Sealed tube
5.3: Heating
With
lithium borohydride; chloro-trimethyl-silane; ammonium acetate; potassium carbonate; acetic acid; trichlorophosphate;
In
tetrahydrofuran; dimethyl sulfoxide;
5.2: Vilsmeier-Haack formylation;
DOI:10.1021/ol1027877
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / dichloromethane; water / 20 °C
2.1: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
2.2: 8 h / 60 °C / Inert atmosphere
3.1: trichlorophosphate / 0.75 h / Cooling with ice
3.2: 0.25 h / 100 °C / Microwave irradiation; Sealed tube
3.3: Heating
With
trifluoroacetic acid; trichlorophosphate;
In
tetrahydrofuran; dichloromethane; water;
3.2: Vilsmeier-Haack formylation;
DOI:10.1021/ol1027877
