(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride

Base Information

Chemical Name:(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride
CAS No.:854669-27-5
Molecular Formula:C₃₅H₅₃FFeN₂
Molecular Weight:576.665
Hs Code.:

(((2,6-di(isopropyl)phenyl)N)2C<sub>3</sub>H-t-Bu<sub>2</sub> iron(II) fluoride

Synonyms:(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride

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Chemical Property of (((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride

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Technology Process of (((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride

There total 1 articles about (((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 415701-49-4
[Fe(methyl)(2,2,6,6-tetramethyl-3,5-bis(2,6-diisopropylphenylimido)hept-4-yl)]

: 420-60-0
trimethyltin fluoride

: 854669-27-5
(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride

Guidance literature:: In toluene; (N2), mixed in toluene, heated at 80°C overnight under stirring; evapd.(vac.), washed (pentane), dried (vac.), elem. anal.;
DOI:10.1021/ja042672l

Reference yield: 95.0%

: 3978-81-2
4-tert-butylpyridine

: 854669-27-5
(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride

: 854669-67-3
(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride(4-t-Bu-pyridine)

Guidance literature:: In diethyl ether; (N2), 1 equiv. of ligand added to Fe complex in Et2O; crystd. at -38°C, elem. anal.;
DOI:10.1021/ja042672l

Reference yield: 86.0%

: 3385-94-2
hexamethyldisilathiane

: 854669-27-5
(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride

: 854669-38-8
(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II)(SSiMe₃)

Guidance literature:: In toluene; byproducts: (CH3)3SnF; (N2), mixed wirt L:Fe molar ratio 2:1 in toluene, heated to 80°C,stirred overnight; evapd.(vac.), dissolved (Et2O, crystd. at -38°C, elem. anal.;
DOI:10.1021/ja042672l