3-bromopropionic anhydride

Base Information

• Chemical Name: 3-bromopropionic anhydride
• CAS No.: 112489-79-9
• Molecular Formula: C₆H₈Br₂O₃
• Molecular Weight: 287.936
• Mol file: 112489-79-9.mol

Synonyms:3-bromopropionic anhydride

Chemical Property of 3-bromopropionic anhydride

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 3-bromopropionic anhydride

There total 1 articles about 3-bromopropionic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

(1,2-bis(diphenylphosphino)ethane)Ni(C2H4CO2) + bromine (7726-95-6) → 3-bromopropionic anhydride (112489-79-9) + dibromo[1,2-bis(diphenylphosphino)ethane]nickel(II) (14647-21-3) + [(1,2-bis(diphenylphosphino)ethaneO2)3Ni][NiBr4]

Guidance literature:

In dichloromethane; at -35 - 20 ℃; for 12h; Glovebox;

DOI:10.1002/ejic.201402952

Reference yield:

3-bromopropionic anhydride (112489-79-9) + 4-aminophenylarsenoxide (1122-90-3) → 4-(bromopropionamido)-phenylarsineoxide

Guidance literature:

3-bromopropionic anhydride; 4-aminophenylarsenoxide; In DMF (N,N-dimethyl-formamide);

With hydrogenchloride; In DMF (N,N-dimethyl-formamide); diethyl ether;

With triethylamine; In DMF (N,N-dimethyl-formamide); diethyl ether;

upstream raw materials:

bromine

Refernces