2-(benzyl(4-fluoro-1-oxo-2,3-dihydro-1H-inden-5-yl)amino)-N,N-diethylacetamide

Base Information

Chemical Name:2-(benzyl(4-fluoro-1-oxo-2,3-dihydro-1H-inden-5-yl)amino)-N,N-diethylacetamide
CAS No.:1379666-62-2
Molecular Formula:C₂₂H₂₅FN₂O₂
Molecular Weight:368.451
Hs Code.:

Synonyms:2-(benzyl(4-fluoro-1-oxo-2,3-dihydro-1H-inden-5-yl)amino)-N,N-diethylacetamide

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Chemical Property of 2-(benzyl(4-fluoro-1-oxo-2,3-dihydro-1H-inden-5-yl)amino)-N,N-diethylacetamide

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Technology Process of 2-(benzyl(4-fluoro-1-oxo-2,3-dihydro-1H-inden-5-yl)amino)-N,N-diethylacetamide

There total 9 articles about 2-(benzyl(4-fluoro-1-oxo-2,3-dihydro-1H-inden-5-yl)amino)-N,N-diethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

: 1379666-61-1
5-(benzylamino)-4-fluoro-2,3-dihydro-1H-inden-1-one

: 78258-15-8
N,N-diethyl-2-iodoacetamide

: 1379666-62-2
2-(benzyl(4-fluoro-1-oxo-2,3-dihydro-1H-inden-5-yl)amino)-N,N-diethylacetamide

Guidance literature:: With caesium carbonate; In acetonitrile; at 20 ℃; for 48h; Reflux;

Reference yield:

: 1379666-58-6
(E)-3-(3-acetamido-6-chloro-2-fluorophenyl)acrylic acid

: 1379666-62-2
2-(benzyl(4-fluoro-1-oxo-2,3-dihydro-1H-inden-5-yl)amino)-N,N-diethylacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; palladium on activated charcoal; hydrogen / methanol / 50 °C / 760.05 Torr

2: polyphosphoric acid / 2 h / 120 °C

3: sulfuric acid / sulfuric acid / 0.5 h / 80 °C

4: caesium carbonate / acetonitrile / 48 h / Reflux

5: caesium carbonate / acetonitrile / 48 h / 20 °C / Reflux

With sulfuric acid; palladium on activated charcoal; hydrogen; caesium carbonate; triethylamine; In methanol; sulfuric acid; acetonitrile;

Reference yield:

: 1379666-59-7
3-(3-acetamido-2-fluorophenyl)propanoic acid

: 1379666-62-2
2-(benzyl(4-fluoro-1-oxo-2,3-dihydro-1H-inden-5-yl)amino)-N,N-diethylacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: polyphosphoric acid / 2 h / 120 °C

2: sulfuric acid / sulfuric acid / 0.5 h / 80 °C

3: caesium carbonate / acetonitrile / 48 h / Reflux

4: caesium carbonate / acetonitrile / 48 h / 20 °C / Reflux

With sulfuric acid; caesium carbonate; In sulfuric acid; acetonitrile;