tert-butyldimethylsilyl (5R,6S)-5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>octanoate

Base Information

Chemical Name:tert-butyldimethylsilyl (5R*,6S*)-5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>octanoate
CAS No.:107036-40-8
Molecular Formula:C₃₈H₆₆O₄Si₃
Molecular Weight:671.196
Hs Code.:

Synonyms:tert-butyldimethylsilyl (5R*,6S*)-5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>octanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyldimethylsilyl (5R*,6S*)-5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>octanoate

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Technology Process of tert-butyldimethylsilyl (5R*,6S*)-5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>octanoate

There total 3 articles about tert-butyldimethylsilyl (5R*,6S*)-5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>octanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl 6-hydroxy-5,6-bis(4-methoxyphenyl)octanoate

: 107036-40-8
tert-butyldimethylsilyl (5R*,6S*)-5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>octanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 45.5 percent / H₂, perchloric acid / Pd/C / acetic acid / 2250.2 Torr

2: 93 percent / BBr₃ / CH₂Cl₂ / 3.5 h / Ambient temperature

3: imidazole / dimethylformamide / 12 h / Ambient temperature

With 1H-imidazole; perchloric acid; hydrogen; boron tribromide; palladium on activated charcoal; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00127a023

Reference yield:

: 107036-38-4,120578-47-4,120578-48-5
(5S*,6R*)-5,6-bis(4-methoxyphenyl)-1-octanoic acid

: 107036-40-8
tert-butyldimethylsilyl (5R*,6S*)-5,6-bis<4-(tert-butyldimethylsiloxy)phenyl>octanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / BBr₃ / CH₂Cl₂ / 3.5 h / Ambient temperature

2: imidazole / dimethylformamide / 12 h / Ambient temperature

With 1H-imidazole; boron tribromide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00127a023