2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside

Base Information

Chemical Name:2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside
CAS No.:1194397-69-7
Molecular Formula:C₈₀H₁₃₃N₅O₁₅
Molecular Weight:1404.96
Hs Code.:

2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside

Synonyms:2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside

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Chemical Property of 2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside

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Technology Process of 2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside

There total 1 articles about 2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 91681-56-0
(3R)-3-dodecanoyloxytetradecanoic acid

: 1194397-66-4
2-azidoethyl 2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl-(1→6)-2-amino-4-O-benzyl-2-deoxy-β-D-glucopyranoside

: 1194397-69-7
2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside

Guidance literature:: (3R)-3-dodecanoyloxytetradecanoic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 1h;

2-azidoethyl 2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl-(1→6)-2-amino-4-O-benzyl-2-deoxy-β-D-glucopyranoside; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1039/c4ob00390j

Reference yield: 87.3%

: 143-07-7
lauric acid

: 1194397-69-7
2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside

: 1194397-71-1
2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-3-O-dodecanoyl-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-3-O-dodecanoyl-β-D-glucopyranoside

Guidance literature:: lauric acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 0.333333h;

2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside; With dmap; In dichloromethane; at 45 ℃;
DOI:10.1039/b907351e

Reference yield: 77.0%

: (R)-3-(benzyloxy)dodecanoic acid

: 1194397-69-7
2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside

: 1608489-14-0
2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido][(R)-3-(benzyloxy)dodecanoyl]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido][(R)-3-(benzyloxy)dodecanoyl]-β-D-glucopyranoside

Guidance literature:: (R)-3-benzyloxy-dodecanoic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 1h;

2-azidoethyl 4,6-O-benzylidene-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranosyl-(1→6)-4-O-benzyl-2-deoxy-2-[(R)-3-(dodecanoyloxy)tetradecanamido]-β-D-glucopyranoside; With dmap; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1039/c4ob00390j