2-<<3-<4-(diphenylmethoxy)-1-piperidinyl>propionyl>amino>-4-methylphenol

Base Information

• Chemical Name: 2-<<3-<4-(diphenylmethoxy)-1-piperidinyl>propionyl>amino>-4-methylphenol
• CAS No.: 157020-44-5
• Molecular Formula: C₂₈H₃₂N₂O₃
• Molecular Weight: 444.574

Synonyms:2-<<3-<4-(diphenylmethoxy)-1-piperidinyl>propionyl>amino>-4-methylphenol

Chemical Property of 2-<<3-<4-(diphenylmethoxy)-1-piperidinyl>propionyl>amino>-4-methylphenol

Chemical Property:

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Technology Process of 2-<<3-<4-(diphenylmethoxy)-1-piperidinyl>propionyl>amino>-4-methylphenol

There total 2 articles about 2-<<3-<4-(diphenylmethoxy)-1-piperidinyl>propionyl>amino>-4-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4-diphenylmethoxypiperidine (58258-01-8) + 2-(acryloylamino)-4-methylphenol (91950-00-4) → 2-<<3-<4-(diphenylmethoxy)-1-piperidinyl>propionyl>amino>-4-methylphenol (157020-44-5)

Guidance literature:

In ethanol; for 2h; Heating;

DOI:10.1021/jm00039a010

Reference yield:

3-amino-4-hydroxytoluene (95-84-1) → 2-<<3-<4-(diphenylmethoxy)-1-piperidinyl>propionyl>amino>-4-methylphenol (157020-44-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1.5 h / 0 °C

2: 75 percent / ethanol / 2 h / Heating

With triethylamine; In ethanol; dichloromethane;

DOI:10.1021/jm00039a010

Reference yield: 57.0%

2-<<3-<4-(diphenylmethoxy)-1-piperidinyl>propionyl>amino>-4-methylphenol (157020-44-5) → 2-[3-(4-benzhydryloxy-1-piperidinyl)propyl]amino-4-methylphenol

Guidance literature:

With dimethylsulfide borane complex; In tetrahydrofuran; for 2h; Heating;

DOI:10.1021/jm00039a010

upstream raw materials:

4-diphenylmethoxypiperidine

2-(acryloylamino)-4-methylphenol

3-amino-4-hydroxytoluene

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