3-(5-(2-fluorophenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid

Base Information

• Chemical Name: 3-(5-(2-fluorophenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid
• CAS No.: 1078723-94-0
• Molecular Formula: C₁₉H₁₇FN₂O₃
• Molecular Weight: 340.354

Synonyms:3-(5-(2-fluorophenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid

Chemical Property of 3-(5-(2-fluorophenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid

Chemical Property:

Purity/Quality:

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Technology Process of 3-(5-(2-fluorophenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid

There total 1 articles about 3-(5-(2-fluorophenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

3-(5-(2-fluorophenyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid (1078723-93-9) + methyl iodide (74-88-4) → 3-(5-(2-fluorophenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid (1078723-94-0)

Guidance literature:

3-(5-(2-fluorophenyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.166667h;

methyl iodide; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/jm800506v

Reference yield:

3-(5-(2-fluorophenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid (1078723-94-0) → 3-(5-(2-fluorophenyl)-1-methyl-7-nitro-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid (1078723-95-1)

Guidance literature:

With sulfuric acid; potassium nitrate; at 20 ℃; for 4h;

DOI:10.1021/jm800506v

upstream raw materials:

3-(5-(2-fluorophenyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid

methyl iodide

Downstream raw materials:

3-(5-(2-fluorophenyl)-1-methyl-7-nitro-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)propanoic acid

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