Technology Process of C17H25ClN2O5S
There total 5 articles about C17H25ClN2O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1: calcium chloride; Sucrose / water / 48 h / 30 °C / Microbiological reaction
2: sodium hydride / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere
3: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
4: triethylamine; dmap / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere
5: hydroxylamine potassium salt / methanol / 48 h / 20 °C
With
dmap; hydroxylamine potassium salt; sodium hydride; triethylamine; trifluoroacetic acid; calcium chloride; Sucrose;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.08.028
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydroxide / chloroform; water / 73 h / 0 - 20 °C
2: potassium tert-butylate / toluene / 1.5 h / -10 - 0 °C / Inert atmosphere
3: calcium chloride; Sucrose / water / 48 h / 30 °C / Microbiological reaction
4: sodium hydride / N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere
5: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
6: triethylamine; dmap / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere
7: hydroxylamine potassium salt / methanol / 48 h / 20 °C
With
dmap; hydroxylamine potassium salt; potassium tert-butylate; sodium hydride; triethylamine; trifluoroacetic acid; calcium chloride; sodium hydroxide; Sucrose;
In
methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.ejmech.2012.08.028
