N-(4-BROMOPHENYL)BUTANAMIDE

Base Information

• Chemical Name: N-(4-BROMOPHENYL)BUTANAMIDE
• CAS No.: 119199-11-0
• Molecular Formula: C10H12BrNO
• Molecular Weight: 242.1124
• Hs Code.: 2924299090
• Mol file: 119199-11-0.mol

Synonyms:CHEMBRDG-BB 5625303;N-(4-BROMOPHENYL)BUTANAMIDE;N-(4-bromophenyl)butanamide(SALTDATA: FREE)

Chemical Property of N-(4-BROMOPHENYL)BUTANAMIDE

Chemical Property:

• Vapor Pressure: 1.01E-05mmHg at 25°C
• Refractive Index: 1.584
• Boiling Point: 371.7 °C at 760 mmHg
• Flash Point: 178.6 °C
• PSA: 29.10000
• Density: 1.409 g/cm³
• LogP: 3.26070

Purity/Quality:

99% ^*data from raw suppliers

N-(4-Bromophenyl)butanamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(4-BROMOPHENYL)BUTANAMIDE

There total 4 articles about N-(4-BROMOPHENYL)BUTANAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

butyryl chloride (141-75-3) + 4-bromo-aniline (106-40-1) → N-(4-bromophenyl)butanamide (119199-11-0)

Guidance literature:

With triethylamine; In dichloromethane; at 5 - 20 ℃;

DOI:10.1021/jm049499o

Reference yield: 88.0%

butanoic acid ethyl ester (105-54-4) + 4-bromo-aniline (106-40-1) → N-(4-bromophenyl)butanamide (119199-11-0)

Guidance literature:

4-bromo-aniline; With TurboGrignard; In tetrahydrofuran; at 20 ℃; for 0.1h; Microreactor;

butanoic acid ethyl ester; In tetrahydrofuran; at 20 ℃; for 0.233333h; Microreactor;

DOI:10.1039/c2gc35037h

Reference yield:

N-phenylbutyramide (1129-50-6) → N-(4-bromophenyl)butanamide (119199-11-0)

Guidance literature:

With 1,2,3,4,5,6-hexabromocyclohexane; In 1,4-dioxane; at 25 ℃; Rate constant; Irradiation;

upstream raw materials:

butyryl chloride

4-bromo-aniline

N-phenylbutyramide

butanoic acid ethyl ester

Downstream raw materials:

6-bromo-2-chloro-3-ethylquinoline

3-ethyl-2-iodoquinolin-6-yl cis-4-methoxycyclohexyl ketone

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