4-nitrobenzene

Base Information

• Chemical Name: 4-nitrobenzene
• CAS No.: 64846-47-5
• Molecular Formula: C₁₀H₄F₆INO₆
• Molecular Weight: 475.04

Synonyms:4-nitrobenzene

Chemical Property of 4-nitrobenzene

Chemical Property:

Purity/Quality:

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Technology Process of 4-nitrobenzene

There total 2 articles about 4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

p-nitrobenzene iodide (636-98-6) + trifluoroacetic acid (76-05-1) → 4-nitrobenzene (64846-47-5)

Guidance literature:

With Oxone; In chloroform; at 20 ℃; for 1.5h;

DOI:10.1021/jo902733f

Reference yield:

p-nitrobenzene iodide (636-98-6) + trifluoroacetic anhydride (407-25-0) → 4-nitrobenzene (64846-47-5)

Guidance literature:

With nitric acid; Nitrogen dioxide;

Reference yield: 92.0%

4-nitrobenzene (64846-47-5) + toluene-4-sulfonic acid (104-15-4) → 4-nitrobenzene (73178-10-6)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1002/mrc.1260270902

upstream raw materials:

p-nitrobenzene iodide

trifluoroacetic anhydride

trifluoroacetic acid

Downstream raw materials:

1-iodyl-4-nitrobenzene

4-nitrobenzene

p-Bis-(acetoxy)-iodylnitrobenzol

C₁₄H₄F₁₂INO₁₀

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