3-[3-(biphenyl-4-yloxymethyl)-pent-4-enyl]-3H-benzo[d][1,2,3]triazin-4-one

Base Information

Chemical Name:3-[3-(biphenyl-4-yloxymethyl)-pent-4-enyl]-3H-benzo[d][1,2,3]triazin-4-one
CAS No.:336107-56-3
Molecular Formula:C₂₅H₂₃N₃O₂
Molecular Weight:397.477
Hs Code.:

3-[3-(biphenyl-4-yloxymethyl)-pent-4-enyl]-3<i>H</i>-benzo[<i>d</i>][1,2,3]triazin-4-one

Synonyms:3-[3-(biphenyl-4-yloxymethyl)-pent-4-enyl]-3H-benzo[d][1,2,3]triazin-4-one

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Chemical Property of 3-[3-(biphenyl-4-yloxymethyl)-pent-4-enyl]-3H-benzo[d][1,2,3]triazin-4-one

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Technology Process of 3-[3-(biphenyl-4-yloxymethyl)-pent-4-enyl]-3H-benzo[d][1,2,3]triazin-4-one

There total 4 articles about 3-[3-(biphenyl-4-yloxymethyl)-pent-4-enyl]-3H-benzo[d][1,2,3]triazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 90-16-4
1,2,3-benzotriazin-4(3H)-one

: 336107-47-2
3-(biphenyl-4-yloxymethyl)-pent-4-en-1-ol

: 336107-56-3
3-[3-(biphenyl-4-yloxymethyl)-pent-4-enyl]-3H-benzo[d][1,2,3]triazin-4-one

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/S0960-894X(00)00646-6

Reference yield:

: 92-69-3
4-Phenylphenol

: 336107-56-3
3-[3-(biphenyl-4-yloxymethyl)-pent-4-enyl]-3H-benzo[d][1,2,3]triazin-4-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: K₂CO₃ / 96 h / 20 °C

1.2: N(nBu)4OAc / acetone / Heating

1.3: 51 percent / MeOH; NaOH / 12 h / 20 °C

2.1: 87 percent / 12 h / Heating

3.1: 95 percent / LAH / diethyl ether / 48 h / -78 °C

4.1: 95 percent / PPh₃; DIAD / tetrahydrofuran / 0 - 20 °C

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; diethyl ether; 2.1: Claisen rearrangement / 4.1: Mitsunobu substitution;
DOI:10.1016/S0960-894X(00)00646-6

Reference yield:

: (E)-4-(Biphenyl-4-yloxy)-but-2-en-1-ol

: 336107-56-3
3-[3-(biphenyl-4-yloxymethyl)-pent-4-enyl]-3H-benzo[d][1,2,3]triazin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / 12 h / Heating

2: 95 percent / LAH / diethyl ether / 48 h / -78 °C

3: 95 percent / PPh₃; DIAD / tetrahydrofuran / 0 - 20 °C

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; diethyl ether; 1: Claisen rearrangement / 3: Mitsunobu substitution;
DOI:10.1016/S0960-894X(00)00646-6