Technology Process of C30H35N3O2
There total 6 articles about C30H35N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
1.2: 0.33 h
1.3: -78 - 20 °C
2.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
trifluoroacetic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: thionyl chloride / 0.5 h / 20 - 60 °C
2.1: hydrogen; palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr
3.1: acetic acid / dichloromethane / 2 h / 20 °C
3.2: 40 °C
4.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
4.2: 0.33 h
4.3: -78 - 20 °C
5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
thionyl chloride; palladium 10% on activated carbon; hydrogen; acetic acid; trifluoroacetic acid; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane;