2-((5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)methoxy)acetonitrile

Base Information

Chemical Name:2-((5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)methoxy)acetonitrile
CAS No.:1018690-41-9
Molecular Formula:C₁₇H₁₃F₂N₃OS
Molecular Weight:345.373
Hs Code.:

Synonyms:2-((5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)methoxy)acetonitrile

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Chemical Property of 2-((5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)methoxy)acetonitrile

Chemical Property:

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Technology Process of 2-((5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)methoxy)acetonitrile

There total 5 articles about 2-((5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)methoxy)acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1018690-40-8
2-(2-oxo-2-phenyl-ethoxy)acetonitrile

: 1018690-17-9
2,5-difluorothiobenzoyl hydrazide; hydrochloride

: 1018690-41-9
2-((5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)methoxy)acetonitrile

Guidance literature:: With potassium acetate; In ethanol; at 20 ℃; for 16h;

Reference yield:

: 1018690-39-5
2-(2-oxo-2-phenyl-ethoxy)acetic acid chloride

: 1018690-41-9
2-((5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)methoxy)acetonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: ammonia / tetrahydrofuran / 2.08 h / -78 - 20 °C

2: pyridine; trifluoroacetic anhydride / 3 h / 0 °C

3: potassium acetate / ethanol / 16 h / 20 °C

With pyridine; ammonia; potassium acetate; trifluoroacetic anhydride; In tetrahydrofuran; ethanol;

Reference yield:

: 1018690-38-4
2-(2-oxo-2-phenyl-ethoxy)acetamide

: 1018690-41-9
2-((5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)methoxy)acetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; trifluoroacetic anhydride / 3 h / 0 °C

2: potassium acetate / ethanol / 16 h / 20 °C

With pyridine; potassium acetate; trifluoroacetic anhydride; In ethanol;