Technology Process of C11H16O2
There total 5 articles about C11H16O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
methanol; Dimethyl ether; water;
for 0.166667h;
Reflux;
DOI:10.1021/ja4018122
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: magnesium chloride; triethylamine / acetonitrile / 0.25 h / 20 °C
1.2: 3 h / Reflux
2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C
2.2: 1 h / 20 °C
3.1: sodium tetrahydroborate / methanol / 0.25 h / 0 °C
4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C
4.2: 11 h / 0 - 20 °C
5.1: hydrogenchloride / methanol; water; Dimethyl ether / 0.17 h / Reflux
With
hydrogenchloride; sodium tetrahydroborate; sodium hydride; triethylamine; magnesium chloride;
In
methanol; Dimethyl ether; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1021/ja4018122
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C
1.2: 1 h / 20 °C
2.1: sodium tetrahydroborate / methanol / 0.25 h / 0 °C
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C
3.2: 11 h / 0 - 20 °C
4.1: hydrogenchloride / methanol; water; Dimethyl ether / 0.17 h / Reflux
With
hydrogenchloride; sodium tetrahydroborate; sodium hydride;
In
methanol; Dimethyl ether; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja4018122
