3-(5-allyl-2,2-dimethyl-4,6-dioxo[1,3]dioxan-5-ylmethyl)benzoic acid methyl ester

Base Information

Chemical Name:3-(5-allyl-2,2-dimethyl-4,6-dioxo[1,3]dioxan-5-ylmethyl)benzoic acid methyl ester
CAS No.:891201-29-9
Molecular Formula:C₁₈H₂₀O₆
Molecular Weight:332.353
Hs Code.:

Synonyms:3-(5-allyl-2,2-dimethyl-4,6-dioxo[1,3]dioxan-5-ylmethyl)benzoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(5-allyl-2,2-dimethyl-4,6-dioxo[1,3]dioxan-5-ylmethyl)benzoic acid methyl ester

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Technology Process of 3-(5-allyl-2,2-dimethyl-4,6-dioxo[1,3]dioxan-5-ylmethyl)benzoic acid methyl ester

There total 1 articles about 3-(5-allyl-2,2-dimethyl-4,6-dioxo[1,3]dioxan-5-ylmethyl)benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 106-95-6
allyl bromide

: 476469-27-9
3-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylmethyl)benzoic acid methyl ester

: 891201-29-9
3-(5-allyl-2,2-dimethyl-4,6-dioxo[1,3]dioxan-5-ylmethyl)benzoic acid methyl ester

Guidance literature:: 3-(2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylmethyl)benzoic acid methyl ester; With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In acetonitrile; at 75 ℃; for 0.333333h;

allyl bromide; In acetonitrile; at 75 ℃; for 5h;
DOI:10.1021/jm051019l

Reference yield:

: 891201-29-9
3-(5-allyl-2,2-dimethyl-4,6-dioxo[1,3]dioxan-5-ylmethyl)benzoic acid methyl ester

: 2-allyl-2-(3-carboxy-benzyl)-malonic acid

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; at 100 ℃; for 3h;
DOI:10.1021/jm051019l

Reference yield:

: 891201-29-9
3-(5-allyl-2,2-dimethyl-4,6-dioxo[1,3]dioxan-5-ylmethyl)benzoic acid methyl ester

: 891201-30-2
3-(2-carboxy-pent-4-enyl)-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / dioxane / 3 h / 100 °C

2: dimethylsulfoxide / 3 h / 130 °C

With sodium hydroxide; In 1,4-dioxane; dimethyl sulfoxide;
DOI:10.1021/jm051019l