C₂₆H₄₂O₄

Base Information

• Chemical Name: C₂₆H₄₂O₄
• CAS No.: 1395502-05-2
• Molecular Formula: C₂₆H₄₂O₄
• Molecular Weight: 418.617
• Mol file: 1395502-05-2.mol

Synonyms:C₂₆H₄₂O₄

Chemical Property of C₂₆H₄₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₄₂O₄

There total 2 articles about C₂₆H₄₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

4-allylguaiacol (97-53-0) + methyl 16-octadecenoic acid ester (17257-44-2,42199-41-7,56554-49-5) → C26H42O4 (1395502-05-2)

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 40 - 45 ℃; for 26h; Inert atmosphere;

DOI:10.1007/s11746-012-2015-0

Reference yield:

methyl 17-hydroxystearate (2380-14-5) → C26H42O4 (1395502-05-2)

Guidance literature:

Multi-step reaction with 2 steps

1: copper sulfate/silica reagent / toluene / 24 h / Reflux

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 26 h / 40 - 45 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; copper sulfate/silica reagent; In dichloromethane; toluene;

DOI:10.1007/s11746-012-2015-0

Reference yield: 69.0%

methyl 17-hydroxystearate (2380-14-5) + C26H42O4 (1395502-05-2) → C45H78O6 (1395502-07-4)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; Inert atmosphere;

DOI:10.1007/s11746-012-2015-0

upstream raw materials:

4-allylguaiacol

methyl 16-octadecenoic acid ester

methyl 17-hydroxystearate

Downstream raw materials:

C₄₅H₇₈O₆