(E)-2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylic acid

Base Information

Chemical Name:(E)-2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylic acid
CAS No.:1207106-17-9
Molecular Formula:C₁₇H₂₀O₃S
Molecular Weight:304.41
Hs Code.:

Synonyms:(E)-2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylic acid

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Technology Process of (E)-2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylic acid

There total 1 articles about (E)-2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 745052-95-3
ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

: 1207106-17-9
(E)-2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylic acid

: 1397795-28-6
2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylic acid

Guidance literature:: With Triphenylphosphine oxide; sodium hydroxide; In ethanol; water; at 60 ℃; for 2.5h; Overall yield = 84 %; Overall yield = 124 g; Inert atmosphere;
DOI:10.1021/op300139g

Reference yield:

: 1207106-17-9
(E)-2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylic acid

: 1001327-35-0
C₁₇H₂₂O₃S

Guidance literature:: With C₃₂H₁₂BF₂₄^(1-)*C₄₀H₄₄IrNOP⁽¹⁺⁾; hydrogen; triethylamine; In methanol; at 30 - 50 ℃; for 20h; under 22801.5 Torr; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/b919902k