ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Base Information

Chemical Name:ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate
CAS No.:745052-95-3
Molecular Formula:C₁₉H₂₄O₃S
Molecular Weight:332.464
Hs Code.:

Synonyms:ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Suppliers and Price of ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

There total 4 articles about ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 745052-94-2
ethyl 2-(4-cyclopropylsulfanylphenyl)-2-oxoacetate

: 745052-95-3
ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Guidance literature:: triphenyl((tetrahydro-2H-pyran-4-yl)methyl)phosphonium iodide; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 1h;

ethyl 2-(4-cyclopropylsulfanylphenyl)-2-oxoacetate; In tetrahydrofuran; at 0 - 20 ℃; for 17.0833h;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 1h; pH=6;

Reference yield:

: 876063-40-0
(4-cyclopropylsulfonylphenyl)-2-oxo-acetic acid ethyl ester

: 745052-95-3
ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Guidance literature:: triphenyl((tetrahydro-2H-pyran-4-yl)methyl)phosphonium iodide; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 1h;

(4-cyclopropylsulfonylphenyl)-2-oxo-acetic acid ethyl ester; In tetrahydrofuran; at 0 - 20 ℃; for 17.0833h;

Reference yield:

: 745052-94-2
ethyl 2-(4-cyclopropylsulfanylphenyl)-2-oxoacetate

: 745052-92-0
triphenyl((tetrahydro-2H-pyran-4-yl)methyl)phosphonium iodide

: 745052-95-3
ethyl 2-(4-(cyclopropylthio)phenyl)-3-(tetrahydro-2H-pyran-4-yl)acrylate

Guidance literature:: triphenyl((tetrahydro-2H-pyran-4-yl)methyl)phosphonium iodide; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Large scale reaction;

ethyl 2-(4-cyclopropylsulfanylphenyl)-2-oxoacetate; In tetrahydrofuran; at 0 - 20 ℃; Large scale reaction;
DOI:10.1021/op300053a