1-[6-(tert-butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-ynyloxymethyl]-4-methoxy-benzene

Base Information

• Chemical Name: 1-[6-(tert-butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-ynyloxymethyl]-4-methoxy-benzene
• CAS No.: 808771-24-6
• Molecular Formula: C₂₉H₅₂O₄Si₂
• Molecular Weight: 520.9

Synonyms:1-[6-(tert-butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-ynyloxymethyl]-4-methoxy-benzene

Chemical Property of 1-[6-(tert-butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-ynyloxymethyl]-4-methoxy-benzene

Chemical Property:

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Technology Process of 1-[6-(tert-butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-ynyloxymethyl]-4-methoxy-benzene

There total 2 articles about 1-[6-(tert-butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-ynyloxymethyl]-4-methoxy-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(4-methoxybenzyloxy)propyne (4039-83-2) → 1-[6-(tert-butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-ynyloxymethyl]-4-methoxy-benzene (808771-24-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / BuLi; BF₃*OEt₂ / tetrahydrofuran

2: 88 percent / 2,6-lutidine / CH₂Cl₂

With 2,6-dimethylpyridine; n-butyllithium; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.tetlet.2004.09.162

Reference yield:

tert-butyldimethylsilyl (R)-glycidyl ether (124150-87-4) → 1-[6-(tert-butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-ynyloxymethyl]-4-methoxy-benzene (808771-24-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / BuLi; BF₃*OEt₂ / tetrahydrofuran

2: 88 percent / 2,6-lutidine / CH₂Cl₂

With 2,6-dimethylpyridine; n-butyllithium; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.tetlet.2004.09.162

Reference yield: 93.0%

1-[6-(tert-butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-ynyloxymethyl]-4-methoxy-benzene (808771-24-6) → 1-[(Z)-(R)-6-(tert-Butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-enyloxymethyl]-4-methoxy-benzene (808771-40-6)

Guidance literature:

With quinoline; hydrogen; Pd-CaCO₃-Pb(OAc)2; In hexane;

DOI:10.1016/j.tetlet.2004.09.162

upstream raw materials:

3-(4-methoxybenzyloxy)propyne

tert-butyldimethylsilyl (R)-glycidyl ether

Downstream raw materials:

1-[(Z)-(R)-6-(tert-Butyl-dimethyl-silanyloxy)-5-triisopropylsilanyloxy-hex-2-enyloxymethyl]-4-methoxy-benzene

(R)-5-[(Z)-4-(4-Methoxy-benzyloxy)-but-2-enyl]-4-methyl-5H-furan-2-one

(Z)-(R)-7-(4-Methoxy-benzyloxy)-3-triisopropylsilanyloxy-hept-5-en-2-ol

(Z)-(R)-7-(4-Methoxy-benzyloxy)-3-triisopropylsilanyloxy-hept-5-en-2-one

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