hexyl(phenylethynyl)sulfane

Base Information

Chemical Name:hexyl(phenylethynyl)sulfane
CAS No.:1269800-67-0
Molecular Formula:C₁₄H₁₈S
Molecular Weight:218.363
Hs Code.:

Synonyms:hexyl(phenylethynyl)sulfane

Suppliers and Price of hexyl(phenylethynyl)sulfane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexyl(phenylethynyl)sulfane

Chemical Property:

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Technology Process of hexyl(phenylethynyl)sulfane

There total 4 articles about hexyl(phenylethynyl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 111-31-9
Hexanethiol

: 1483-82-5
phenylethynyl chloride

: potassium hydride

: 1269800-67-0
hexyl(phenylethynyl)sulfane

Guidance literature:: Hexanethiol; potassium hydride; In tetrahydrofuran; mineral oil; at 50 ℃; for 0.25h; Inert atmosphere;

phenylethynyl chloride; With dimethyl amine; In tetrahydrofuran; mineral oil; at -40 - 20 ℃; Inert atmosphere;
DOI:10.1039/c5ob00494b

Reference yield: 67.0%

: 111-31-9
Hexanethiol

: 536-74-3
phenylacetylene

: 1269800-67-0
hexyl(phenylethynyl)sulfane

Guidance literature:: With Ni₂P nanoparticles on N,P-codoped carbon; air; In N,N-dimethyl-formamide; at 50 ℃; for 4h; Schlenk technique; Glovebox;
DOI:10.1039/c9gc04137k

Reference yield: 62.0%

: 111-31-9
Hexanethiol

: C₁₂H₁₅NO₂S

: 1269800-67-0
hexyl(phenylethynyl)sulfane

Guidance literature:: Hexanethiol; With potassium hydride; In tetrahydrofuran; at 20 - 30 ℃; for 0.5h; Inert atmosphere;

C₁₂H₁₅NO₂S; With dimethyl amine; In tetrahydrofuran; at -40 - 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/jo500814y