N-cyclohexyl-2-oxoheptanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone

Base Information

Chemical Name:N-cyclohexyl-2-oxoheptanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone
CAS No.:78257-88-2
Molecular Formula:C₂₈H₄₇N₃O₃S
Molecular Weight:505.765
Hs Code.:

Synonyms:N-cyclohexyl-2-oxoheptanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cyclohexyl-2-oxoheptanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone

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Technology Process of N-cyclohexyl-2-oxoheptanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone

There total 4 articles about N-cyclohexyl-2-oxoheptanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 39085-59-1
trisylhydrazine

: 81470-96-4
2-Oxo-heptanoic acid cyclohexylamide

: 78257-88-2
N-cyclohexyl-2-oxoheptanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone

Guidance literature:: hydrogenchloride;
DOI:10.1016/S0040-4020(01)93267-3

Reference yield:

: 931-53-3
Cyclohexyl isocyanide

: 78257-88-2
N-cyclohexyl-2-oxoheptanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 65 degC, 50 min., 2.) aq. acetone, 0 degC to 25 degC, 2 h

2: 85 percent / conc. HCl

hydrogenchloride;
DOI:10.1016/S0040-4020(01)93267-3

Reference yield:

: 142-61-0
Hexanoyl chloride

: 78257-88-2
N-cyclohexyl-2-oxoheptanamide 2,4,6-tri-iso-propylbenzenesulphonylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 65 degC, 50 min., 2.) aq. acetone, 0 degC to 25 degC, 2 h

2: 85 percent / conc. HCl

hydrogenchloride;
DOI:10.1016/S0040-4020(01)93267-3