1,3,4,5,6,11a-hexahydro-7E-2-benzothionine

Base Information

Chemical Name:1,3,4,5,6,11a-hexahydro-7E-2-benzothionine
CAS No.:211427-69-9
Molecular Formula:C₁₂H₁₆S
Molecular Weight:192.325
Hs Code.:

Synonyms:1,3,4,5,6,11a-hexahydro-7E-2-benzothionine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,4,5,6,11a-hexahydro-7E-2-benzothionine

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Technology Process of 1,3,4,5,6,11a-hexahydro-7E-2-benzothionine

There total 3 articles about 1,3,4,5,6,11a-hexahydro-7E-2-benzothionine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trans-2-phenyl-1-[(trimethylsilyl)methyl]tetrahydrothiopyranium perchlorate

: 97416-71-2
(E)-5-methylsulfanyl-1-phenylpent-1-ene

: 211427-69-9
1,3,4,5,6,11a-hexahydro-7E-2-benzothionine

: 5,7,8,9,10,11-Hexahydro-6-thia-benzocyclononene

Guidance literature:: With cesium fluoride; In dimethyl sulfoxide; at 25 ℃; for 3h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1039/a802309c

Reference yield:

: trans-2-phenyl-1-[(trimethylsilyl)methyl]tetrahydrothiopyranium perchlorate

: 97416-71-2
(E)-5-methylsulfanyl-1-phenylpent-1-ene

: 5-methylsulfanyl-1-phenylpentan-1-one

: 211427-69-9
1,3,4,5,6,11a-hexahydro-7E-2-benzothionine

: 5,7,8,9,10,11-Hexahydro-6-thia-benzocyclononene

Guidance literature:: With cesium fluoride; In dimethyl sulfoxide; at 25 ℃; for 24h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1039/a802309c

Reference yield:

: trans-2-phenyl-1-[(trimethylsilyl)methyl]tetrahydrothiopyranium perchlorate

: 1622-06-6
2-phenyl-tetrahydro-thiopyran

: 97416-71-2
(E)-5-methylsulfanyl-1-phenylpent-1-ene

: 5-methylsulfanyl-1-phenylpentan-1-one

: 211427-69-9
1,3,4,5,6,11a-hexahydro-7E-2-benzothionine

: 5,7,8,9,10,11-Hexahydro-6-thia-benzocyclononene

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; cesium fluoride; In 1,2-dimethoxyethane; at 0 ℃; for 24h; Product distribution; other solvent, temperatures and reaction time;
DOI:10.1039/a802309c