E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride

Base Information

Chemical Name:E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride
CAS No.:953394-08-6
Molecular Formula:C₃₀H₃₃N₃O₄*ClH
Molecular Weight:536.071
Hs Code.:

Synonyms:E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride

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Chemical Property of E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride

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Technology Process of E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride

There total 2 articles about E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 953394-07-5
D-N-(4-[1,3]Dioxolan-2-yl-2,5-dimethylphenyl)acrylamide

: 171722-92-2
4-piperidyl N-(2-biphenyl)carbamate

: 953394-08-6
E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride

Guidance literature:: D-N-(4-[1,3]Dioxolan-2-yl-2,5-dimethylphenyl)acrylamide; 4-piperidyl N-(2-biphenyl)carbamate; In ethanol; dichloromethane; at 45 - 50 ℃; for 18h;

With hydrogenchloride; water; In ethanol; dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 953394-10-0
biphenyl-2-ylcarbamic acid 1-[2-(4-[1,3]dioxolan-2-yl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl ester

: 953394-08-6
E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride

Guidance literature:: With hydrogenchloride; water; In ethanol; dichloromethane; for 3h;

Reference yield:

: 953394-08-6
E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride

: 953393-95-8
N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt

: 953394-01-9
biphenyl-2-ylcarbamic acid 1-[2-(4-{[(R)-2-(tert-butyldimethylsilanyloxy)-2-(3-formylamino-4-hydroxyphenyl)ethylamino]methyl}-2,5-dimethylphenylcarbamoyl)-ethyl]piperidin-4-yl ester

Guidance literature:: E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride; N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt; In methanol; dichloromethane; at 20 ℃; for 3h;

With sodium tris(acetoxy)borohydride; In methanol; dichloromethane; at 0 - 20 ℃; for 2.16667h;

With sodium hydrogencarbonate; In methanol; dichloromethane; water; at 0 ℃; Product distribution / selectivity;