N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt

Base Information

Chemical Name:N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt
CAS No.:953393-95-8
Molecular Formula:C₂H₄O₂*C₁₅H₂₆N₂O₃Si
Molecular Weight:370.521
Hs Code.:

Synonyms:N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt

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Chemical Property of N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt

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Technology Process of N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt

There total 1 articles about N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 953393-96-9
N-{5-[(R)-2-benzylamino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-benzyloxyphenyl}formamide

: 64-19-7,77671-22-8
acetic acid

: 953393-95-8
N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt

Guidance literature:: With hydrogen; 20% Pd(OH)2 on carbon; In methanol; at 20 ℃; for 10h;

Reference yield:

: 953394-00-8
E-Biphenyl-2-ylcarbamic Acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester

: 953393-95-8
N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt

: biphenyl-2-ylcarbamic acid 1-[2-(4-{[(R)-2-(tert-butyldimethylsilanyloxy)-2-(3-formylamino-4-hydroxyphenyl)ethylimino]methyl}-2,5-dimethyl-phenylcarbamoyl)ethyl]piperidin-4-yl ester

Guidance literature:: In methanol; at 45 - 50 ℃; for 1h;

Reference yield:

: 953394-08-6
E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride

: 953393-95-8
N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt

: 953394-01-9
biphenyl-2-ylcarbamic acid 1-[2-(4-{[(R)-2-(tert-butyldimethylsilanyloxy)-2-(3-formylamino-4-hydroxyphenyl)ethylamino]methyl}-2,5-dimethylphenylcarbamoyl)-ethyl]piperidin-4-yl ester

Guidance literature:: E-Biphenyl-2-ylcarbamic acid 1-[2-(4-Formyl-2,5-dimethylphenylcarbamoyl)ethyl]piperidin-4-yl Ester Hydrochloride; N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}-formamide acetic acid salt; In methanol; dichloromethane; at 20 ℃; for 3h;

With sodium tris(acetoxy)borohydride; In methanol; dichloromethane; at 0 - 20 ℃; for 2.16667h;

With sodium hydrogencarbonate; In methanol; dichloromethane; water; at 0 ℃; Product distribution / selectivity;