(1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzenemethanol-α,α,-d2

Base Information

Chemical Name:(1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzenemethanol-α,α,-d2
CAS No.:1351704-13-6
Molecular Formula:C₁₄H₁₆O₂
Molecular Weight:218.264
Hs Code.:

Synonyms:(1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzenemethanol-α,α,-d2

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Chemical Property of (1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzenemethanol-α,α,-d2

Chemical Property:

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Technology Process of (1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzenemethanol-α,α,-d2

There total 3 articles about (1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzenemethanol-α,α,-d2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1351704-18-1
(1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2,2-dimethyl-4H-1,3-benzodioxin-4-one

: 1351704-15-8
(1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzaldehyde-α-d

: 1351704-13-6
(1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzenemethanol-α,α,-d2

Guidance literature:: With lithium aluminium deuteride; In tetrahydrofuran; at -78 ℃; for 3h;
DOI:10.1002/ejoc.201100771

Reference yield:

: 1351704-17-0
(1E,3E,5E)-tributylhepta-1,3,5-trienylstannane

: 1351704-15-8
(1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzaldehyde-α-d

: 1351704-13-6
(1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzenemethanol-α,α,-d2

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; lithium chloride / N,N-dimethyl-formamide / 36 h / 20 °C

2: lithium aluminium deuteride / tetrahydrofuran / 3 h / -78 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium aluminium deuteride; trifuran-2-yl-phosphane; lithium chloride; In tetrahydrofuran; N,N-dimethyl-formamide; 1: Stille coupling;
DOI:10.1002/ejoc.201100771

Reference yield:

: 164014-40-8
2,2-dimethyl-5-trifluoromethylsulfonyloxy-4H-(1,3)benzodioxin-4-one

: 1351704-15-8
(1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzaldehyde-α-d

: 1351704-13-6
(1'E,3'E,5'E)-6-(hepta-1',3',5'-trienyl)-2-hydroxybenzenemethanol-α,α,-d2

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; lithium chloride / N,N-dimethyl-formamide / 36 h / 20 °C

2: lithium aluminium deuteride / tetrahydrofuran / 3 h / -78 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium aluminium deuteride; trifuran-2-yl-phosphane; lithium chloride; In tetrahydrofuran; N,N-dimethyl-formamide; 1: Stille coupling;
DOI:10.1002/ejoc.201100771