10-(4-iodo-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4]benzodiazepine

Base Information

• Chemical Name: 10-(4-iodo-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4]benzodiazepine
• CAS No.: 473264-08-3
• Molecular Formula: C₂₀H₁₇IN₂O₂
• Molecular Weight: 444.272

Synonyms:10-(4-iodo-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4]benzodiazepine

Chemical Property of 10-(4-iodo-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4]benzodiazepine

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Technology Process of 10-(4-iodo-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4]benzodiazepine

There total 2 articles about 10-(4-iodo-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4]benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-lodo-2-methoxybenzoic acid + 3-methyl-N-(3-methylbutyl)-1-butanamine (544-00-3) + 2-methoxy-4-iodobenzoic acid (89942-34-7) + 10,11-dihydro-5H-benzo[e]pyrrolo[1,2-a][1,4]diazepine (22162-53-4) → 10-(4-iodo-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4]benzodiazepine (473264-08-3)

Guidance literature:

In thionyl chloride; hexane; dichloromethane; ethyl acetate; toluene;

Reference yield:

3-methyl-N-(3-methylbutyl)-1-butanamine (544-00-3) + 2-methoxy-4-iodobenzoic acid (89942-34-7) + 10,11-dihydro-5H-benzo[e]pyrrolo[1,2-a][1,4]diazepine (22162-53-4) → 10-(4-iodo-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4]benzodiazepine (473264-08-3)

Guidance literature:

In thionyl chloride; hexane; dichloromethane; ethyl acetate; toluene;

Reference yield:

10-(4-iodo-2-methoxybenzoyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4]benzodiazepine (473264-08-3) + 2-Methylphenylboronic acid (16419-60-6) → (10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-[3-methoxy-2'-methyl-[1,1'-biphenyl]-4-yl]-methanone (473264-09-4)

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine)palladium ⁽⁰⁾; In ethanol; hexane; water; ethyl acetate; toluene;

upstream raw materials:

3-methyl-N-(3-methylbutyl)-1-butanamine

2-methoxy-4-iodobenzoic acid

10,11-dihydro-5H-benzo[e]pyrrolo[1,2-a][1,4]diazepine

Downstream raw materials:

(10,11-dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-[3-methoxy-2'-methyl-[1,1'-biphenyl]-4-yl]-methanone

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