4,7,10-tris(p-tolylsulfonyl)-4,7,10-triaza-1,13-bis<(tetrahydropyran-2-yl)oxy>tridecane

Base Information

Chemical Name:4,7,10-tris(p-tolylsulfonyl)-4,7,10-triaza-1,13-bis<(tetrahydropyran-2-yl)oxy>tridecane
CAS No.:77416-54-7
Molecular Formula:C₄₁H₅₉N₃O₁₀S₃
Molecular Weight:850.132
Hs Code.:

Synonyms:4,7,10-tris(p-tolylsulfonyl)-4,7,10-triaza-1,13-bis<(tetrahydropyran-2-yl)oxy>tridecane

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Chemical Property of 4,7,10-tris(p-tolylsulfonyl)-4,7,10-triaza-1,13-bis<(tetrahydropyran-2-yl)oxy>tridecane

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Technology Process of 4,7,10-tris(p-tolylsulfonyl)-4,7,10-triaza-1,13-bis<(tetrahydropyran-2-yl)oxy>tridecane

There total 3 articles about 4,7,10-tris(p-tolylsulfonyl)-4,7,10-triaza-1,13-bis<(tetrahydropyran-2-yl)oxy>tridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 52601-80-6
N,N’,N”-tris(p-toluenesulfonyl)diethylenetriamine N,N-disodium salt

: 77416-52-5
1-(methanesulfonoxy)-3-<(tetrahydropyran-2-yl)oxy>-propane

: 77416-54-7
4,7,10-tris(p-tolylsulfonyl)-4,7,10-triaza-1,13-bis<(tetrahydropyran-2-yl)oxy>tridecane

Guidance literature:: In N,N-dimethyl-formamide; at 95 ℃; for 2h;
DOI:10.1021/jo00342a007

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 77416-54-7
4,7,10-tris(p-tolylsulfonyl)-4,7,10-triaza-1,13-bis<(tetrahydropyran-2-yl)oxy>tridecane

Guidance literature:: Multi-step reaction with 3 steps

1: conc. HCl

2: N(C₂H₅)3 / CH₂Cl₂ / 0.5 h / -5 °C

3: 90 percent / dimethylformamide / 2 h / 95 °C

With hydrogenchloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00342a007

Reference yield:

: 2162-33-6
3-(tetrahydropyran-2-yloxy)propan-1-ol

: 77416-54-7
4,7,10-tris(p-tolylsulfonyl)-4,7,10-triaza-1,13-bis<(tetrahydropyran-2-yl)oxy>tridecane

Guidance literature:: Multi-step reaction with 2 steps

1: N(C₂H₅)3 / CH₂Cl₂ / 0.5 h / -5 °C

2: 90 percent / dimethylformamide / 2 h / 95 °C

With triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00342a007